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Volumn , Issue 26, 2007, Pages 4298-4300

The structure of the first supramolecular α-cyclodextrin complex with an aliphatic monofunctional carboxylic acid

Author keywords

Cyclodextrins; Inclusion compounds; Pseudochannel structure; X ray diffraction

Indexed keywords

EID: 34548712437 PISSN: 1434193X EISSN: 10990690 Source Type: Journal
DOI: 10.1002/ejoc.200700454 Document Type: Article

Times cited : (25)

References (18)

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- Single crystals of complex 1 instantaneously undergo desolvation; a colorless platelet of approximate dimensions 0.40X0.15 X 0.03 mm3 was covered with a thin layer of vacuum grease, rapidly mounted in a cryo loop and immediately exposed to a cold stream of N2. The structure was solved by dual space methods as implemented in SHELXD;[11] the best solution was associated with a correlation coefficient of 79.85 and allowed to locate most atoms of the eight symmetrically independent cyclodextrin moieties. The structure model was completed by difference Fourier syntheses and refined on F2 with SHELXL.[12] Resolution of the diffraction data and accuracy of geometric parameters are limited, and no H atoms could be associated with the solvent molecules. No attempt was made to refine part of the structure model with anisotropic displacement parameters, and no split positions for water oxygen were assigned. H atoms associated wi
- 1 = 0.1566 (21017 observed data). S = 1.108. CCDC-634928 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.

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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.