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Crystal data for 3·1.5 pentane: C71.5H 106,Cr2N4, Mr, 1125.60, 0.35 x 0.25 x 0.15 mm3, triclinic, space group P1, a, 13.308(7, b, 13.368(7, c, 19.253(10) Å, α, 102.741(5, β, 105.688(5, γ, 89.970(5)°, V, 3210(3) Å3, Z, 2, ρcalcd, 1.165 g cm -3, μ, 0.382 mm-1, MoKα radiation, λ, 0.71073 Å, T, 120(2) K, 2θmax, 56.56°, 35 508 reflections, 14 514 independent, Rint, 0.0777. R, 0.0552, wR, 0.1434, largest difference peak and hole: 0.753 and -0.380 e Å-3. Hydrogen atom H1 was the largest peak in the penultimate difference map and yielded computationally stable results of isotropic refinement. The data set was treated with SQUEEZE A. L. Spek, J. App
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