GC-MS analysis of acylated derivatives of the side-chain regioisomers of 4-methoxy-3-methyl-phenethylamines related to methylenedioxymethamphetamine

Journal of Chromatographic Science

Volumn 45, Issue 8, 2007, Pages 477-485

  Awad, Tamer ^a   Clark, C Randall ^a   DeRuiter, Jack ^a  

^a AUBURN UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

3,4 METHYLENEDIOXYMETHAMPHETAMINE; PHENETHYLAMINE DERIVATIVE;

ACYLATION; ARTICLE; CHEMISTRY; MASS FRAGMENTOGRAPHY; STEREOISOMERISM;

ACYLATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; N-METHYL-3,4-METHYLENEDIOXYAMPHETAMINE; PHENETHYLAMINES; STEREOISOMERISM;

EID: 34548564593     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/45.8.477     Document Type: Article

References (14)

1. L. Aalberg, J. DeRuiter, F.T. Noggle, E. Sippola, and C.R. Clark. Chromatographic and mass spectral methods of identification for the side-chain and ring regioisomers of methylenedioxymethamphetamine. J. Chromatogr. Sci. 38: 329-37 (2000).
2. L. Aalberg, J. DeRuiter, F.T. Noggle, E. Sippola, and C. R. Clark, Chromatographic and spectroscopic methods of identification for the side chain regioisomers of 3,4-methylenedioxyphenethylamines related to MDEA, MDMMA and MBDB. J. Chromatogr. Sci. 41: 227-33 (2003).
3. L. Aalberg, J. DeRuiter, E. Sippola, and C.R. Clark. Gas chromatographic optimization studies on the side chain and ring regioisomers of methylenedioxymethamphetamine. J. Chromatogr. Sci. 42: 293-98 (2004).
4. T. Awad, J. DeRuiter, and C.R. Clark. GC-MS analysis of acylated derivatives of the side chain and ring regioisomers of methylenedioxymethamphetamine. J. Chromatogr. Sci. 43: 296-303 (2005).
5. T. Awad, C.R. Clark, and J. DeRuiter. Chromatographic and mass spectral studies on methoxy methyl methamphetamines related to 3,4- methylenedioxymethamphetamine. J. Chromatogr. Sci. 45: 222-22 (2007).
6. J. DeRuiter, P.L. Holsten, C.R. Clark, and F.T. Noggle. Liquid chromatographic and mass spectral methods of identification for the regioisomeric 2,3- and 3,4-methylenedioxyphenalkylamines. J. Chromatogr. Sci. 36: 131-38 (1998).
7. C.R. Clark, F.T. Noggle, and J. DeRuiter. Chromatographic and mass spectrometric methods for the differentiation of N-methyl-1-(3,4- methylenedioxyphenyl)-2-butanamine from regioisomeric derivatives. J. Chromatogr. Sci. 34: 230-37 (1996).
8. T. Awad, C.R. Clark, and J. DeRuiter. Chromatographic and mass spectral studies on methoxymethcathinones related to 3,4-methylenedioxymethamphetamine. J. Chromatogr. Sci. 44: 155-61 (2006).
9. W.H. Soine, R.E. Shark, and D.T. Agee. Differentiation of 2,3-methylene-dioxyamphetamine from 3,4-methylenedioxyamphetamine. J. Forensic Sci. 28: 386-90 (1983).
10. D.E. Nichols, A.J. Hoffman, R.A. Oberlender, P. Jacob III, and A.T. Shulgin. Derivatives of 1-(1,3-benzodioxolyl)-2-butanamine: representatives of a novel therapeutic class. J. Med. Chem. 29: 2009-15 (1986).
11. J.F. Casale, P.A. Hays, and R.F.X. Klein. Synthesis and characterization of the 2,3-methylenedioxyamphetamines. J. Forensic Sci. 40: 391-400 (1995).
12. F.W. McLafferty and F. Turecek. Interpretation of Mass Spectra, 4th ed. University Science Books, Sausalito, California, 1993, p 275.
13. C.R. Clark, A.K. Valaer, F.T. Noggle, and J DeRuiter, GC-MS analysis of acylated derivatives of methamphetamine and regioisomeric phenethylamines. J. Chromatogr. Sci. 33: 485 (1995).
14. D.T. Stafford, H.S. Nichols, and W.H. Anderson. Efficiency of capillary column GC in separating LSD and lysergic acid methylpropylamide (LAMPA). J. Forensic Sci. 29: 291-98 (1984).