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Volumn 54, Issue 3, 2007, Pages 583-585

Synthesis of a novel type of phosphates of puerarin

Author keywords

Atherton Todd reaction; Chemoselectivity; Phosphates; Puerarin

Indexed keywords

EID: 34548544898 PISSN: 00094536 EISSN: None Source Type: Journal
DOI: 10.1002/jccs.200700084 Document Type: Article

Times cited : (5)

References (13)

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- Spectra data of 3a: 31P NMR (400 MHz, 20 °C, DMSO-d6, δ ppm, 6.93, 7.90 (1P, 13C-NMR (400 MHz, 20 °C, DMSO-d6, δ ppm, δ 153.73, 153.73 (C-2, 122.12, 121.55 (C-3, 175.07, 174.98 (C-4, 127.06, 126.96 (C-5, 117.17, 117.01 (C-6, 153.51, 153.16 (C-7, 118.78, 118.69 (C-8, 155.79, 155.07 (C-8a, 120.43, 120.43 (C-4a, 123.83, 123.74 (C-1′, 130.27, 130.19 C-2, 6′, 115.23, 115.23 (C-3′, 5′, 157.59, 157.54 (C-4′, 74.24, 73.08 (C-1″, 71.12, 70.85 (C-2″) 79.34, 78.88 (C-3″, 70.69, 70.47 (C-4″, 82.63, 82.27 (C-5″, 61.72, 61.61 (C-6″, 65.00, 64.94 (C-OCH2, 16.10, 16.04 (C-CH3, 1H-NMR (400 MHz, 20 °C, DMSO-d6, δ ppm, δ 8.50, 8.49 (1H, s, C2-H, 8.17, 8.16 (1H, d, C5-H, J, 8.9 Hz, 7.52, 7.46 1H, d, C6-H, J, 9.0 Hz, 7.43, 7.42
- +; Elemental analyses, (Cal. %): C 54.14 (54.35), H 5.27 (5.29), P 5.63 (5.61); m.p. 159-161 °C.

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