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Compared to the solution IR spectra, the IR spectra of the crystaline solids measured as KBr disks, display additional signals at lower energy which can be attributed to semi-bridging COs (2a: 2048 s, 1993 sh, 1981 s, 1967 s, 1917 m, 1899 m, 1877 w; 3a: 2054 m, 2034 s, 1991 s, 1976 s, 1963 m, 1944 s, 1884 m, 1872 m; not measured for Te-containing clusters).
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Compared to the solution IR spectra, the IR spectra of the crystaline solids measured as KBr disks, display additional signals at lower energy which can be attributed to semi-bridging COs (2a: 2048 s, 1993 sh, 1981 s, 1967 s, 1917 m, 1899 m, 1877 w; 3a: 2054 m, 2034 s, 1991 s, 1976 s, 1963 m, 1944 s, 1884 m, 1872 m; not measured for Te-containing clusters).
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G. M. Sheldrick, SHELXL-97, Universität Göttingen, 1997.
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(b) G. M. Sheldrick, SHELXL-97, Universität Göttingen, 1997.
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