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Volumn 36, Issue 8, 2007, Pages 1010-1011

Molecular structures of the coloring species of a leuco dye with phenolic color developers

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EID: 34548303563     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.2007.1010     Document Type: Article
Times cited : (21)

References (19)
  • 1
    • 34548345096 scopus 로고    scopus 로고
    • For review of the leuco dyes, see: Chemistry and Applications of Leuco Dyes, ed. by R. Muthyala, Plenum Press, New York and London, 1997.
    • For review of the leuco dyes, see: Chemistry and Applications of Leuco Dyes, ed. by R. Muthyala, Plenum Press, New York and London, 1997.
  • 2
    • 34548335008 scopus 로고    scopus 로고
    • S. Machida, S. Takayama, N. Ikeda, T. Urano, K. Sano, Proceedings of 218th ACS National Meeting, New Orleans, LA, U.S.A., August, 1999, Abstr., No. ENVR-135.
    • a) S. Machida, S. Takayama, N. Ikeda, T. Urano, K. Sano, Proceedings of 218th ACS National Meeting, New Orleans, LA, U.S.A., August, 1999, Abstr., No. ENVR-135.
  • 3
    • 34548333933 scopus 로고    scopus 로고
    • N. Ikeda, S. Takayama, S. Machida, T. Urano, A. Tanaka, M. Oguchi, T. Nomaki, K. Sano, Proceedings of 220th ACS National Meeting, Washington, DC, U.S.A., August, 2000, Abstr., No. IEC-181.
    • b) N. Ikeda, S. Takayama, S. Machida, T. Urano, A. Tanaka, M. Oguchi, T. Nomaki, K. Sano, Proceedings of 220th ACS National Meeting, Washington, DC, U.S.A., August, 2000, Abstr., No. IEC-181.
  • 14
    • 34548333929 scopus 로고    scopus 로고
    • Synthesis and isolation of 2: Rhodamine B base was purchased from Sigma-Aldrich Corp. and purified by recrystallization from toluene. Ethyl-3,4,5-trihydroxybenzoate was purchased from Tokyo Chemical Industry Co, Ltd. and used as received. Rhodamine B base (45.7 mg, 0.10 mmol) and ethyl-3,4,5-trihydroxybenzoate (20.0 mg, 0.10 mmol) were placed in a screw vial (20 cm3) and acetonitrile (1 cm3) was added. The mixture was shaken for a few minutes, and dark red solution was immediately obtained. The solution was kept for an hour with the solvent removed under ambient temperature and red blocks were precipitated. The precipitates were separated by decantation and the solvent was removed completely in vacuo, giving red crystals of 2 22.0 mg, 0.034 mmol, 34% yield, For syntheses and isolation of 3 and 4, see Supporting Information which is available electronically on the CSJ-Journal web site
    • 3) was added. The mixture was shaken for a few minutes, and dark red solution was immediately obtained. The solution was kept for an hour with the solvent removed under ambient temperature and red blocks were precipitated. The precipitates were separated by decantation and the solvent was removed completely in vacuo, giving red crystals of 2 (22.0 mg, 0.034 mmol, 34% yield). For syntheses and isolation of 3 and 4, see Supporting Information which is available electronically on the CSJ-Journal web site, http://www.csj.jp/journals/chem-lett/index.html.
  • 17
    • 0345140750 scopus 로고
    • ed. by A. J. C. Wilson, Kluwer Academic Publishers, Dordrecht
    • International Tables for Crystallography, ed. by A. J. C. Wilson, Kluwer Academic Publishers, Dordrecht, 1992, vol. C, pp. 692-700.
    • (1992) International Tables for Crystallography , vol.100 , pp. 692-700


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.