Preparation of (S)-2-(2-chloro-1-hydroxyethyl)thiophene by lipase-catalyzed resolution in organic phase

Chinese Journal of Organic Chemistry

Volumn 27, Issue 7, 2007, Pages 857-861

  Xu, Gang ^a   Chen, Yong Mei ^a   Wu, Jian Ping ^a   Yang, Li Rong ^a  

^a ZHEJIANG UNIVERSITY   (China)

Author keywords

(s) 2 (2 Chloro 1 hydroxyethyl)thiophene; Duloxetine; Lipase catalyzed; Resolution

Indexed keywords

EID: 34548299613     PISSN: 02532786     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (16)

1. Ghoniem, G. M. J. Urol. 2005, 173, 1647.
2. Zinner, N. R. Eur. Urol., Suppl. 2005, 4(1), 29.
3. Andersson, K. E.; Schroeder, A. Drug Discovery Today 2004, 9, 259.
4. Kamal, A.; Khanna, G. B. R.; Ramu, R.; Krishnaji, T. Tetrahedron Lett. 2003, 44, 4783.
5. Vidal, V. R.; Girard, C.; Touati, R.; Tranchier, J. P.; Hassine, B. B.; Genêt, J. P. Adv. Synth. Catal. 2003, 345, 261.
6. Liu, D.; Gao, W. Z.; Wang, C. J.; Zhang, X. M. Angew. Chem., Int. Ed. 2005, 44, 1687.
7. Hamada, T.; Torii, T.; Izawa, K.; Ikariya, T. Tetrahedron 2004, 60, 7411.
8. Andrew, M. R. US 6008412, 1999 [Chem. Abstr. 2000, 133, 1429P].
9. (a) Dietmar, R.; Perea, A. WO 03070720, 2003 [Chem. Abstr. 2005, 143, 6440P].
10. (b) Borghese, A. WO 03062219, 2003 [Chem. Abstr. 2004, 141, 9172P].
11. (a) Azerad, R. Bull. Soc. Chim. Fr. 1995, 132, 17.
12. (b) Wong, C. H.; Halcomb, R. L.; Ichikawa, Y.; Kajimoto, T. Angew. Chem., Int. Ed. Engl. 1995, 34, 412.
13. Sun, F. L.; Xu, G.; Wu, J. P.; Yang, L. R. Tetrahedron: Asymmetry 2006, 17, 2907.
14. (a) Roberts, S. M. J. Chem. Soc., Perkin Trans. 1 1999, 1.
15. (b) Leuenberger, H. G. W. Pure Appl. Chem. 1990, 62, 752.
16. Zhang, J.; Wu, J. P.; Yang, L. R. J. Mol. Catal. B: Enzym. 2004, 31, 67.