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Volumn 46, Issue 17, 2007, Pages 7215-7223

Preparation, characterization, and structural systematics of diphosphane and diarsane complexes of gallium(III) halides

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EID: 34548250860     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic700895r     Document Type: Article
Times cited : (36)

References (44)
  • 2
    • 0011056377 scopus 로고
    • Wilkinson, G, Gillard, R. D, McCleverty, J. A, Eds, Pergamon: Oxford, U.K
    • Taylor, M. J. In Comprehensive Coordination Chemistry; Wilkinson, G., Gillard, R. D., McCleverty, J. A., Eds.; Pergamon: Oxford, U.K., 1987; Vol. 3, pp 105-152.
    • (1987) Comprehensive Coordination Chemistry , vol.3 , pp. 105-152
    • Taylor, M.J.1
  • 4
    • 22444447093 scopus 로고    scopus 로고
    • McCleverty, J. A, Meyer, T. J, Eds, Elsevier: Oxford, U.K
    • Robinson, G. H. In Comprehensive Coordination Chemistry II; McCleverty, J. A., Meyer, T. J., Eds.; Elsevier: Oxford, U.K., 2004; Vol. 3, pp 347-382.
    • (2004) Comprehensive Coordination Chemistry II , vol.3 , pp. 347-382
    • Robinson, G.H.1
  • 5
    • 84902433467 scopus 로고    scopus 로고
    • McCleverty, J. A, Meyer, T. J, Eds, Elsevier: Oxford, U.K
    • O'Brien, P.; Pickett, N. L. In Comprehensive Coordination Chemistry II; McCleverty, J. A., Meyer, T. J., Eds.; Elsevier: Oxford, U.K., 2004; Vol. 9, pp 1005-1063.
    • (2004) Comprehensive Coordination Chemistry II , vol.9 , pp. 1005-1063
    • O'Brien, P.1    Pickett, N.L.2
  • 15
    • 34548220326 scopus 로고    scopus 로고
    • ibid, 1967, 45, 3187-3192.
    • ibid, 1967, 45, 3187-3192.
  • 32
    • 34548292320 scopus 로고    scopus 로고
    • 2 solution).
    • 2 solution).
  • 33
    • 34548290689 scopus 로고    scopus 로고
    • Tetrahedral [GaX4, show one IR active stretch (ν3, t2) and two Raman active stretches (ν1, a1 and ν3, t2, Literature values (cm-1) are X, Cl ν1, 346, ν3, 386; X, Br ν1, 210, ν3, 278; X, I ν1, 145, ν3, 222. Data from Nakamoto, K. IR Spectra of Inorganic and Coordination Compounds, 2nd ed, Wiley: New York, 1970
    • 3 = 222. Data from Nakamoto, K. IR Spectra of Inorganic and Coordination Compounds, 2nd ed.; Wiley: New York, 1970.
  • 37
    • 34548259749 scopus 로고    scopus 로고
    • 1 (No. 31) (both in the standard setting). A solution in the centrosymmetric Pmmn readily emerged with the cation having mirror symmetry, but two of the aromatic carbon atoms showed very elongated displacement ellipsoids perpendicular to the plane of the ring (R1 ≈ 0.10). This suggested the lower symmetry solution, but attempts here gave unsatisfactory refinement and no improvement to the model. Although the chemical identity is not in doubt, the structure is not presented here.
    • 1 (No. 31) (both in the standard setting). A solution in the centrosymmetric Pmmn readily emerged with the cation having mirror symmetry, but two of the aromatic carbon atoms showed very elongated displacement ellipsoids perpendicular to the plane of the ring (R1 ≈ 0.10). This suggested the lower symmetry solution, but attempts here gave unsatisfactory refinement and no improvement to the model. Although the chemical identity is not in doubt, the structure is not presented here.


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