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34548292320
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2 solution).
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2 solution).
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33
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34548290689
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Tetrahedral [GaX4, show one IR active stretch (ν3, t2) and two Raman active stretches (ν1, a1 and ν3, t2, Literature values (cm-1) are X, Cl ν1, 346, ν3, 386; X, Br ν1, 210, ν3, 278; X, I ν1, 145, ν3, 222. Data from Nakamoto, K. IR Spectra of Inorganic and Coordination Compounds, 2nd ed, Wiley: New York, 1970
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34548259749
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1 (No. 31) (both in the standard setting). A solution in the centrosymmetric Pmmn readily emerged with the cation having mirror symmetry, but two of the aromatic carbon atoms showed very elongated displacement ellipsoids perpendicular to the plane of the ring (R1 ≈ 0.10). This suggested the lower symmetry solution, but attempts here gave unsatisfactory refinement and no improvement to the model. Although the chemical identity is not in doubt, the structure is not presented here.
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1 (No. 31) (both in the standard setting). A solution in the centrosymmetric Pmmn readily emerged with the cation having mirror symmetry, but two of the aromatic carbon atoms showed very elongated displacement ellipsoids perpendicular to the plane of the ring (R1 ≈ 0.10). This suggested the lower symmetry solution, but attempts here gave unsatisfactory refinement and no improvement to the model. Although the chemical identity is not in doubt, the structure is not presented here.
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