FTIR-spectroscopic characterization of humic acids and humin fractions obtained by advanced NaOH, Na4P2O7, and Na 2CO3 extraction procedures

Journal of Plant Nutrition and Soil Science

Volumn 170, Issue 4, 2007, Pages 522-529

  Tatzber, Michael ^a   Stemmer, Michael ^b   Spiegel, Heide ^b   Katzlberger, Christian ^b   Haberhauer, Georg ^c   Mentler, Axel ^a   Gerzabek, Martin H ^a  

^a UNIVERSITY OF NATURAL RESOURCES AND LIFE SCIENCES   (Austria)

^b AUSTRIAN AGENCY FOR HEALTH AND FOOD SAFETY   (Austria)

^c ARC SEIBERSDORF RESEARCH GMBH   (Austria)

Author keywords

E4:E 6; FA:HA ratio; FTIR spectroscopy; HA extractions; Humin fraction

Indexed keywords

EID: 34548094081     PISSN: 14368730     EISSN: 15222624     Source Type: Journal    
DOI: 10.1002/jpln.200622082     Document Type: Article

References (31)

1. Capriel, P., Beck, T., Borchert, H., Gronholz, J., Zachmann, G. (1995): Hydrophobicity of the organic matter in arable soils. Soil Boil. Biochem. 27, 1453-1458.
2. 13C and FTIR signatures. Geoderma 128, 28-37.
3. Eusterhues, K., Rumpel, C., Kleber, M., Kögel-Knabner, I. (2003): Stabilisation of soil organic matter by interactions with minerals as revealed by mineral dissolution and oxidative degradation. Org. Geochem. 34, 1591-1600.
4. Francioso, O., Ciavatta, C., Tugnoli, V., Sanchez-Cortes, S., Gessa, C. (1998): Spectroscopic characterization of pyrophosphate incorporation during extraction of peat humic acids. Soil Sc. Soc. Am. J. 62, 181-187.
5. García, C., Hernandez, T. (1996): Organic matter in bare soils of the Mediterranean region with a semiarid climate. Arid Soil Res. Rehabil. 10, 31-41.
6. Gerzabek, M. H. (1991): Criteria for compost maturity - methods for organic substances characterization. OEFZS report Nr. 4584, Hauptabteilung Agrarforschung und Biotechnologie, Österreichisches Forschungszentrum Seibersdorf, A-2444 Seibersdorf, pp. 1-10.
7. Gerzabek, M. H., Mohamad, S. A., Danneberg, O. H., Schaffer, K. (1992): Heavy metals in humic substances from a town refuse and a refuse-sewage sludge compost. Die Bodenkultur 43, 21-27.
8. Gerzabek, M. H., Danneberg, O. H., Kandeler, E. (1993): Bestimmung des Humifizierungsgrades, in: Schinner, F., Öhlinger, R., Kandeler, E., Margesin, R. (eds.): Bodenbiologische Arbeitsmethoden. Springer, Berlin, pp. 107-110.
9. Gerzabek, M. H., Pichlmayer, F., Kirchmann, H., Haberhauer, G. (1997): The response of soil organic matter to manure amendments in a long-term experiment at Ultuna, Sweden. Eur. J. Soil Sci. 48, 273-282.
10. Haberhauer, G., Gerzabek, M. H. (1999): Drift and transmission FT-IR spectroscopy of forest soils: an approach to determine decomposition processes of forest litter. Vibr. Spectr. 19, 413-417.
11. Haberhauer, G., Rafferty, B., Strebl, F., Gerzabek, M. H. (1998): Comparison of the composition of forest soil litter derived from three different sites at various decompositial stages using FTIR spectroscopy. Geoderma 83, 331-342.
12. Haberhauer, G., Feigl, B., Gerzabek, M. H., Cerri, C. (2000): FT-IR spectroscopy of organic matter in tropical soils: Changes induced through deforestation. Appl. Spectr. 54, 221-224.
13. Head, M. J., Zhou, W. J. (2000): Evaluation of NaOH leaching techniques to extract humic acids from paleosols. Nucl. Instr. Meth. Phys. Res. B 172, 434-439.
14. Hesse, M., Meier, H., Zeeh, B. (2005): Spektroskopische Methoden in der organischen Chemie. Thieme, Stuttgart, pp. 33-69.
15. Kaiser, M., Ellerbrock, R. H. (2005): Functional characterization of soil organic matter fractions different in solubility originating from a long-term field experiment. Geoderma 127, 196-206.
16. Novotny, E. H., Blum, W. E. H., Gerzabek, M. H., Mangrich, A. S. (1999): Soil management system effects on size fractionated humic substances. Geoderma 92, 87-109.
17. 13C CPMAS NMR of the de-ashed soil humin in a second-growth Douglas-fir stand of coastal British Columbia. Geoderma 68, 229-241.
18. Rosa, H. A., Oliveira, L. C., Bellin, I. C., Rocha, J. C., Romão, L. P. C., Filho, N. L. D. (2005): Influence of alkaline extraction on the charakteristics of humic substances in Brasilian soils. Thermochim. Acta 433, 81-86.
19. Rumpel, C., Knicker, H., Kögel-Knabner, I., Skjemstad, J. O., Hüttl, R. F. (1998): Types and chemical composition of organic matter in reforested lignite-rich mine soils. Geoderma 86, 123-142.
20. Schnitzer, M., Khan, S. U. (1978): Soil Organic Matter. Elsevier Scientific Publishing Company, Amsterdam, pp. 3-6.
21. Senesi, N., D'Orazio, V., Ricca, G. (2003): Humic acids in the first generation of EUROSOILS. Geoderma 116, 325-344.
22. Sierra, M. M. D., Rauen, T. G., Tormen, L., Debacher, N. A., Soriano-Sierra, E. J. (2005): Evidence from surface tension and fluorescence data of a pyrene-assisted micelle-like assemblage of humic substances. Water Res. 39, 3811-3818.
23. Spiegel, H., Pfeffer, M., Hösch, J. (2002): N-Dynamik bei reduzierter Bodenbewirtschaftung. Arch. Agron. Soil Sci. 48, 503-512.
24. Song, J., Peng, P., Huang, W. (2005): Characterization of humic acid-like material isolated from the humin fraction of a topsoil. Soil Sci. 170, 599-611.
25. Sposito, G. (1989): The Chemistry of Soils. Oxford University Press, Oxford, p. 10.
26. Spaccini, R., Piccolo, A., Haberhauer, G., Stemmer, M., Gerzabek, M. H. (2001): Decomposition of maize straw in three European soils as revealed by DRIFT spectra of soil particle fractions. Geoderma 99, 245-260.
27. Terashima, M., Fukushima, M., Shunitz, T. (2004): Influence of pH on the surface activity of humic acid: micelle-like aggregate formation and interracial adsorption. Coll. Surfaces A 247, 77-83.
28. Vollhardt, K. P. C., Schore, N. E. (1995): Organische Chemie. VCH, Weinheim, pp. 770-777.
29. Wang, M. C., Liu, C. P., Sheu, B. H. (2004): Characterization of organic matter in rainfall, through fall, stemflow, and streamwater from three subtropical forest ecosystems. J. Hydrol. 289, 275-285.
30. Xing, B.-S., Liu, J.-D., Liu, X.-B., Han, X.-Z. (2005): Extraction and characterization of humic acids and humin fractions from a black soil of China. Pedosphere 15, 1-8.
31. Ziechmann, W. (1980): Huminstoffe. Verlag Chemie, Weinheim, p. 188.