Liquid chromatography-tandem mass spectrometric method for determination of the anti-inflammatory compound vicenin-2 in the leaves of L. ericoides Mart

Biomedical Chromatography

Volumn 21, Issue 9, 2007, Pages 925-930

  de Moraes, Solange Leite ^a   Tomaz, José Carlos ^a   Lopes, Norberto Peporine ^a  

^a UNIVERSITY OF SÃO PAULO   (Brazil)

Author keywords

ESI MS MS; LC MS MS; Natural product; Quantification; Vicenin 2

Indexed keywords

ELECTRODEPOSITION; ELECTROSPRAY IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

ANTI-INFLAMMATORIES; ESI-MS-MS; LC-MS-MS; LC.MS/MS; NATURAL PRODUCTS; QUANTIFICATION; RAPID METHOD; SPECTROMETRIC METHODS; TANDEM MASS SPECTROMETRIC; VICENIN-2;

PLANT EXTRACTS;

ACETIC ACID; ACETONITRILE; ANTIINFLAMMATORY AGENT; HERBACEOUS AGENT; LYCHNOPHORA ERICOIDES EXTRACT; MIKANIA GLOMERATA EXTRACT; PLANT EXTRACT; UNCLASSIFIED DRUG; VICENIN 2; WATER;

ARTICLE; ASTERACEAE; CALIBRATION; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; DRUG DETERMINATION; ELECTROSPRAY MASS SPECTROMETRY; LINEAR SYSTEM; LIQUID CHROMATOGRAPHY; LYCHNOPHORA ERICOIDES; MIKANIA; MIKANIA GLOMERATA; NONHUMAN; PHYTOCHEMISTRY; PLANT LEAF; QUANTITATIVE ANALYSIS; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY; VALIDATION PROCESS;

GOOSE PARVOVIRUS;

EID: 34547978000     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.828     Document Type: Article

References (19)

1. Borella JC, Lopes JLC, Vichnewski W, Cunha WR and Herz W. Sesquiterpene lactones, triterpenes and flavone from Lychnophora ericoides and Lychnophora pseudovillosissima. Biochemical Systemic Ecological 1998; 26: 671-676.
2. Borsato MLC, Grael CFF, Souza GEP and Lopes NP. Analgesic activity of the lignans from Lychnophora ericoides. Phytochemistry 2000; 55: 809-813.
3. Bradshaw J, Butina D, Dunn AJ, Green RH, Hajek M, Jones MM, Lindon JC and Sidebotton PJ. A Rapid and facile method for the dereplication of purified natural products. Journal of Natural Products 2001; 64: 1541-1546.
4. Colombo R, Yariwake JH, Queiroz EF, Ndjoko K and Hostettmann K. On-line identification of sugarcane (Saccharum officinarum L.) methoxyflavones by liquid chromatography-UV detection using post-column derivatization and liquid chromatography-mass spectrometry. Journal of Chromatography A 2005; 1082: 51-57.
5. Crotti AEM, Vessecchi R, Lopes JLC and Lopes NP. Espectrometria de massas corn ionização por electrospray: processos químicos envolvidos na formação de íons de substâncias orgânicas de baixo peso molecular. Quimica Nova 2006; 29: 287-292.
6. Cuyckens F and Claeys M. Mass spectrometry in the structural analysis of flavonoid. Journal of Mass Spectrometry 2004; 39: 1-14.
7. Gobbo-Neto L, Santos MD, Kanashiro A, Almeida MC, Lucisano-Valim YM, Lopes JLC, Souza GEP and Lopes NP. Evaluation of the anti-inflammatory and antioxidant activities of di-C-glucosylflavones from Lychnophora ericoides (Asteraceae). Planta Medica 2005; 71: 3-6.
8. Huck CW, Buchmeiser MR and Bonn GK. Fast analysis of flavonoids in plant extracts by liquid chromatography-ultraviolet absorbance detection on poly(carboxylic acid)-coated silica and electrospray ionization tandem mass spectrometric detection. Journal of Chromatography A 2001; 943: 33-38.
9. Lopes NP. Essência da arnica. Revista Fapesp Pesquisa 2001; 64: 42.
10. Maurin AJM, Iamamoto Y, Lopes NP, Smith JRL and Bonato PS. LC-MS-MS identification of drug metabolites obtained by metalloporphyrin mediated oxidation. Journal Brazilian Chemistry Society 2003; 14: 322-328.
11. Moraes SL, Carollo CA, Tomaz JC and Lopes NP. Development and validation of a liquid chromatography mass spectrometry method for the determination of the anti-inflammatory 6,8-di-C-β-D-glucosylapigenin in species of Lychnophora. Analytical Chemistry: An Indian Journal 2007; 4: 1-4.
12. Nielsen KF and Smedsgaard J. Fungal metabolite screening: database of 474 mycotoxins and fungal metabolites for dereplication by standardized liquid chromatography-UV-mass spectrometry methodology. Journal of Chromatography A 2003; 1002: 111-136.
13. Pivatto M, Crotti AEM, Lopes NP, Castro-Gamboaa I, Rezendea A, Viegas C, Young MCM, Furlana M and Bolzani VS. Electrospray ionization mass spectrometry screening of piperidine alkaloids from Senna spectabilis (Fabaceae) extracts: fast identification of new constituents and co-metabolites. Journal of the Brazilian Chemical Society 2005; 16: 1431-1438.
14. Sakamoto HT, Flausino D, Castellano EE, Stark CBW, Gates PJ and Lopes NP. Sesquiterpene lactones from Lychnophora ericoides. Journal of Natural Products 2003; 66: 693-697.
15. Santos MD. Lychnophora ericoides Mart: avaliação farmacológica e considerações sobre o metabolismo oxidativo das substâncias bioativas. Ph.D. Thesis. Universidade de São Paulo, Brazil, 2006.
16. Santos MD, Gobbo-Neto L, Albarella L, Souza GEP and Lopes NP. Analgesic activity of di-caffeoylquinic acids from roots of Lychnophora ericoides (Arnica da serra). Journal of Ethnopharmacology 2005; 96: 545-549.
17. Santos PA, Amarante MFC, Pereira MAS, Bertoni B, França SC, Pessoa C, Moraes MO, Costa-Lotufo LV, Pereira MRP and Lopes NP. Production of an antiproliferative furanoheliangolide by Lychnophora ericoides Cell Culture. Chemical Pharmaceutical Bulletin 2004; 52: 1433-1435.
18. Smyth WF, Joyce C, Ramachandran VN, O'Kane E and Coulter D. Characterization of selected hypnotic drugs and their metabolites using electrospray ionisation with ion trap mass spectrometry and with quadrupole time-of-flight mass spectrometry and their determination by liquid chromatography-electrospray ionization-ion trap mass spectrometry. Analytical Chimica Acta 2004; 506: 203-208.
19. Wolfender JL, Ndjoko K and Hostettmann K. Liquid chromatography with ultraviolet absorbance-mass spectrometric detection and with nuclear magnetic resonance spectroscopy a powerful combination for on-line structural investigation of plant metabolites. Journal of Chromatography A 2003; 1000: 437-455.