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34547834544
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note
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-1): 1632 w, 1599 w, 1577 m, 1523 s, 1431 s, 1355 m, 1244 w, 1220 m, 1156 s, 1105 s, 1040 w, 879 w, 844 s, 727 s, 644 m.
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27
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34547845711
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note
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2 using the SHELXTL 97 crystallographic software package. Anisotropic thermal parameters were used to refine all non-hydrogen atoms. Hydrogen atoms were located from difference Fourier maps.
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