Validation and application of capillary electrophoresis for the analysis of lidocaine in a skin tape stripping study

Biomedical Chromatography

Volumn 21, Issue 8, 2007, Pages 775-779

  Chik, Z ^a   Johnston, A ^b   Tucker, A T ^b   Burn, R T ^b   Perrett, D ^b  

^a UNIVERSITY OF MALAYA   (Malaysia)

^b QUEEN MARY UNIVERSITY OF LONDON   (United Kingdom)

Author keywords

Capillary eleclrophoresis; Lidocaine; Method validation; Tape stripping

Indexed keywords

ELECTROLYTES; FUSED SILICA; QUALITY CONTROL; SIGNAL TO NOISE RATIO; WATER INJECTION;

BACKGROUND ELECTROLYTES; CAPILLARY ELECLROPHORESIS; CAPILLARY-ZONE ELECTROPHORESIS; FUSED-SILICA CAPILLARIES; INTERNAL STANDARDS; LIDOCAINE; METHOD VALIDATIONS; MIGRATION TIME; SIMPLE++; TAPE STRIPPING;

CAPILLARY ELECTROPHORESIS;

ELECTROLYTE; LIDOCAINE; LOCAL ANESTHETIC AGENT; METHANOL; PHOSPHORIC ACID; PROCAINE; SILICON DIOXIDE; WATER;

ACCURACY; ARTICLE; CALIBRATION; CAPILLARY ZONE ELECTROPHORESIS; CONTROLLED STUDY; DRUG DETERMINATION; DRUG ISOLATION; DRUG STRUCTURE; INJECTION; QUALITY CONTROL; SIGNAL NOISE RATIO; SKIN; TEST STRIP; VALIDATION PROCESS;

EID: 34547671035     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.823     Document Type: Article

References (17)

1. Benfeldt E and Groth L. Feasibility of measuring lipophilic or protein-bound drugs in the dermis by in vivo microdialysis after topical or systemic drug administration. Acta Dermato-Venereologica 1998; 78: 274-278.
2. Bo LD, Mazzucchelli P and Marzo A. Highly sensitive bioassay of lidocaine in human plasma by high-performance liquid chromatography-tandem mass spectrometry. Journal of Chromatography A 1999; 854: 3-11.
3. Chik Z, Lee TD, Holt DW, Johnston A and Tucker AT. Validation of high-performance liquid chromatographic-mass spectrometric method for the analysis of lidocaine in human plasma. Journal of Chromatographic Sciences 2006; 44: 262-265.
4. fda. Guidance For Industry: Bioanalytical Method Validation, 2001; http://www.fda.gov/cder/guidance/425fnl.pdf. 2001 (accessed 20 August 2003).
5. Geiser L, Rudaz S and Veuthey JL. Validation of capillary electrophoresis-mass spectrometry methods for the analysis of a pharmaceutical formulation. Electrophoresis 2003; 24: 3049-3056.
6. Geiser L, Rudaz S and Veuthey JL. Decreasing analysis time in capillary electrophoresis: validation and comparison of quantitative performances in several approaches. Electrophoresis 2005; 26: 2293-2302.
7. Kenkel JM, Lipschitz AH, Shepherd G, Armstrong VW, Streit F, Oellerich M, Luby M, Rohrich RJ and Brown SA. Pharmacokinetics and safety of lidocaine and monoethylglycine-xylidide in liposuction: a microdialysis study. Plastic Reconstruction Surgery 2004; 114: 516-524.
8. Kreilgaard M. Dermal pharmacokinetics of microemulsion formulations determined by in vivo microdialysis. Pharmaceutical Research 2001; 18: 367-373.
9. Kreilgaard M, Kemme MI, Burggraaf J, Schoemaker RC and Cohen AF. Influence of a microemulsion vehicle on cutaneous bioequivalence of a lipophilic model drug assessed by microdialysis and pharmacodynamics. Pharmaceutical Research 2001; 18: 593-599.
10. Lotfi H, Debord J, Dreyfuss MF, Marquet P, Ben Rhaiem M, Feiss P and Lachatre G. Simultaneous determination of lidocaine and bupivacaine in human plasma: application to pharmacokinetics. Therapeutic Drug Monitoring 1997; 19: 160-164.
11. Pershing LK, Bakhtian S, Poncelet CE, Corlett JL and Shah VP. Comparison of skin stripping, in vitro release, and skin blanching response methods to measure dose response and similarity of triamcinolone acetonide cream strengths from two manufactured sources. Journal of Pharmaceutical Sciences 2002a; 91: 1312-1323.
12. Pershing LK, Corlett JL and Nelson JL. Comparison of dermatopharmacokinetic vs. clinicial efficacy methods for bioequivalence assessment of miconazole nitrate vaginal cream, 2% in humans. Pharmaceutical Research 2002b; 19:. 270-277.
13. Pershing LK, Nelson JL, Corlett JL, Shrivastava SP, Hare DB and Shah VP. Assessment of dermatopharmacokinetic approach in the bioequivalence determination of topical tretinoin gel products. Journal of American Academy of Dermatology2003; 48: 740-751.
14. Reddy MB, Stinchcomb AL, Guy RH and Bunge AL. Determining dermal absorption parameters in vivo from tape strip data. Pharmaceutical Research 2002; 19:. 292-298.
15. Wang Z, Wan H, Anderson MS, Abdel-Rehim M and Blomberg LG. Separation of lidocaine and its metabolites by capillary electrophoresis using volatile aqueous and nonaqueous electrolyte systems. Electrophoresis 2001; 22: 2495-2502.
16. Watanabe T, Namera A, Yashiki M, Iwasaki Y and Kojima T. Simple analysis of local anaesthetics in human blood using headspace solid-phase microextraction and gas chromatography-mass spectrometry-electron impact ionization selected ion monitoring. Journal of Chromatography B Biomedical Sciences Application 1998; 709:. 225-232.
17. Weigmann H, Lademann J, Pelchrzim R, Sterry W, Hagemeister T, Molzahn R, Schaefer M, Lindscheid M, Schaefer H and Shah VP. Bioavailability of clobetasol propionate-quantification of drug concentrations in the stratum corneum by dermatopharmacokinetics using tape stripping. Skin Pharmacology and Applied Skin Physiology 1999; 12: 46-53.