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Volumn 36, Issue 7, 2007, Pages 938-939

Synthesis and mesomorphism study of novel carbohydrate-derived liquid crystals containing glucosyl and chenodiolyl residues

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EID: 34547369617 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2007.938 Document Type: Article

Times cited : (6)

References (11)

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8
- 34547301718
- Supporting Information is available: The synthetic route of GC4DB; the Synthesis and experimental details; the molecular structure of GC4DB and the X-ray diffraction patterns of quenched GCnDB series.
- Supporting Information is available: The synthetic route of GC4DB; the Synthesis and experimental details; the molecular structure of GC4DB and the X-ray diffraction patterns of quenched GCnDB series.

9
- 34547376836
- Selected physical data of GC4DB are as follows: 1HNMR (300 MHz; CDCl3; Me4Si) δ 1.31 (m, 30H, CH3, 4.09 (m, 20H, CH2-O, 7.14 (d, 20H, J, 5 Hz, O-Ar-COO, 8.15 (d, 20H, J, 1 Hz, O-Ar-COO, 7.16-7.64 (m, 80H, Ar-Ar, 1.58-2.36 (m, 80H, OOC-(CH2)4-COO, 0.93-4.01 (m, 185H, H-chenodiolyl, 4.11 (d, 2H, J, 0.67 Hz, CH2-glucosyl, 4.60-6.66 (m, 5H, CH-glucosyl, 13C NMR (300 MHz; CDCl3; Me4Si) δ 14.61 (10 × q, 63.76 (10 × t, 114.24, 132.27 (40 × d, 121.82, 163.33, 164.89 (30 × s, 122.08, 128.08 (80 × d, 137.89, 150.09, 150.56 (40 × s, 24.17, 33.80, 33.96 (40 × d, 172.21, 173.21 (20 × s, 13.53, 13.36, 19.31 (15 × q, 20.77, 24.86, 28.03, 29.63, 31.23, 31.24, 31.57, 32.46, 35.81, 40.22 (50 × t, 34.75, 37.03, 42.64, 45.36, 49.11, 56.10, 71.35, 73.91 40 ×
- 81: C, 73.20; H, 19.94%. Found: C, 72.90; H, 19.71%.

10
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- Yao, D.S.¹ Zhang, B.Y.² Li, Y.H.³ Xiao, W.Q.⁴

11
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- ed. by I. Dierking, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, Chap. 5, pp
- I. Dierking, in Textures of Liquid Crystals, ed. by I. Dierking, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2003, Chap. 5, pp. 51-70.
- (2003) Textures of Liquid Crystals , pp. 51-70
- Dierking, I.¹

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