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G. Meyer L. R. Morss, editors, Kluwer Academic Publishers, Dordrecht, The Netherlands
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84858108589
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Rb{(Pr6(C)2}I12: C 2I12Pr6Rb (2477.75 g mol-1, diffractometer IPDS-II, Stoe, Darmstadt; Mo-Kα (graphite monochromator, λ, 71.073 pm, T, 293(2) K; 2θmax, 59.5°; 97 images, 0° ≤ ω ≤ 180°, φ, 0°; 0° ≤ φ 14°, φ, 90°; Δω= 2°; indices: -13 ≤ h ≤ 13, 13 ≤ k ≤ 13, 13 ≤ 1 ≤ 13; ρcalc, 5.107 g cm-3; 8243 reflection intensities measured of which 4141 were symmetrically independent, Rint, 0.0821, F(000, 1039, μ, 21.882 mm-1. Triclinic, P1̄ (no. 2, a, 960.1(2, b, 957.0(2, c, 1003.4(2) pm, α, 71.74(2, α, 70.69(2, γ, 72.38(2)°, V, 805.6(3) 106pm3, Z, 1. Structure solution and refinement were carried out using the programs SHELXS-97 and SHELXL-97 G. M. Sheldrick, Pr
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all = 1.108. Further details on the crystal structure determination may be obtained from the Fachinformationszentrum Karlsruhe, 76344 Eggenstein-Leopoldshafen, Germany (fax: (+49)7247-808-666; e-mail: crysdata@fizkarlsruhe.de), on quoting the depository number ICSD-417636, the authors and the journal citation.
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in: Inorg. Chem. in Focus (G. Meyer, D. Naumann, L. Wesemann, eds.), Wiley-VCH, Weinheim, 2006, 3, 1 (chapter 1).
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