SCOPUS 정보 검색 플랫폼

Volumn , Issue 29, 2007, Pages 3103-3105

Tetraplatinum precursors for supramolecular assemblies: Syntheses, crystal structures, and stereoselective self-assemblies of [Pt4(μ- OCOCH3)6(κ4-N4-DArBp)] (DArBp = 1,3-bis(arylbenzamidinate)propane)

(4) Ohashi, Masato a Yagyu, Akihiro a Yamagata, Tsuneaki a Mashima, Kazushi a

a OSAKA UNIVERSITY (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

DICARBOXYLIC ACID DERIVATIVE; PLATINUM DERIVATIVE; PROPANE; TETRAMER;

ARTICLE; CRYSTAL STRUCTURE; DIASTEREOISOMER; PRECURSOR; STEREOCHEMISTRY; SYNTHESIS;

EID: 34447625883 PISSN: 13597345 EISSN: None Source Type: Journal
DOI: 10.1039/b703730a Document Type: Article

Times cited : (27)

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- 1H NMR observation of the crude product of this reaction showed the formation of an unidentified minor by-product. The major product, tetramer 4, was finally isolated by recrystallization from THF-hexane solution. The minor product might be another oligomer (such as dimer) or the other diastereomeric tetramer to be hereinafter described The complex 4 should be represented as ΔΔΔΔ (and its enantiomer ΛΛΛΛ; Scheme 2). Other possible diastereomers of the tetramer are described in the ESI
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- note One of the two acetate signals was observed as multiplet (while the other one was singlet), indicating that the complex 5 is obtained as a mixture of diastereoisomers (See ESI)
- These angle values were calculated from the torsion angle of C(carboxyl)-CEN-CEN′-C′(carboxyl), where CEN and CEN′ represent the centroids of the two cyclopentadienyl rings in the 1,1′-ferrocenedicarboxylic acid

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