Glyoxal sample preparation for high-performance liquid chromatographic detection of 2,4-dinitro-phenylhydrazone derivative: Suppression of polymerization and mono-derivative formation by using methanol medium

Journal of Chromatography A

Volumn 1161, Issue 1-2, 2007, Pages 338-341

  Nakajima, Koichi ^a   Ohta, Kyuji ^a   Mostefaoui, Toufik A ^b   Chai, Wen ^c   Utsukihara, Takamitsu ^d   Horiuchi, C Akira ^d   Murakami, Masahiko ^e  

^a HOSEI UNIVERSITY   (Japan)

^b UNIVERSITY OF MILAN   (Italy)

^c CHANGSHU INSTITUTE OF TECHNOLOGY   (China)

^d RIKKYO UNIVERSITY   (Japan)

^e NIHON UNIVERSITY   (Japan)

Author keywords

DNPH silica cartridge; Glyoxal; Glyoxal sodium bisulfite; Mono derivative formation; Polymerization; Sampling

Indexed keywords

GLYOXAL SODIUM BISULFITE; HYDRAZONE DERIVATIVES; MONO DERIVATIVE FORMATION; SILICA CARTRIDGE;

ALDEHYDES; DERIVATIVES; METHANOL; POLYMERIZATION; SAMPLING; SILICA;

AROMATIC COMPOUNDS;

GLYOXAL; HYDROCHLORIC ACID; METHANOL; PHENYLHYDRAZONE DERIVATIVE;

ARTICLE; CHEMICAL ANALYSIS; DISSOLUTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; POLYMERIZATION; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SAMPLING;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; GLYOXAL; HYDRAZONES; METHANOL; POLYMERS; SPECTROPHOTOMETRY, ULTRAVIOLET;

EID: 34447617850     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2007.06.057     Document Type: Article

References (18)

1. Kean A.J., Grosjean E., Grosjean D., and Hartley R.A. Environ. Sci. Technol. 35 (2001) 4198
2. Grosjean E., Green P.G., and Grosjean D. Anal. Chem. 71 (1999) 1851
3. Tuazon E.C., Leod H.M., Atkinson R., and Carter W.P.L. Environ. Sci. Technol. 20 (1986) 383
4. Atkinson R. Atmos. Environ. 34 (2000) 2063
5. Hatakeyama S., Washida N., and Akimoto H. J. Phys. Chem. 90 (1986) 173
6. Smith D.F., Kleindienst T.E., and Hudgens E.E. J. Chromatogr. 483 (1989) 431
7. Grosjean E., and Grosjean D. Int. J. Environ. Anal. Chem. 61 (1995) 47
8. Druzik C.M., Grosjean D., Neste A.V., and Parmar S.S. Int. J. Environ. Anal. Chem. 38 (1990) 495
9. METHOD 8315A Determination of Carbonyl Compounds by High Performance Liquid Chromatography (HPLC), U.S. Environmental Protection Agency, 1996.
10. Determination of Formaldehyde in Ambient Air Using Adsorbent Cartridge Followed by High Performance Liquid Chromatography (HPLC), U.S. Environmental Protection Agency, EPA/625/R-96/010b, 1999.
11. Pacolay B.D., Ham J.E., and wells J.R. J. Chromatogr. A 1131 (2006) 275
12. M. Windholz (Ed.), The Merck Index, 10th ed., Merck, Rahway, 1983.
13. Cole A.R.H., and Osborne G.A. Spectrochim. Acta 27A (1971) 2461
14. Harris R.K. Spectrochim. Acta 20 (1964) 1129
15. Uchiyama S., Matsushima E., Tokunaga H., Otsubo Y., and Ando M. J. Chromatogr. A 1116 (2006) 165
16. Harries C., and Temme P. Ber. Dtsch. Chem. Ges. 40 (1907) 165
17. Zurek G., and Karst U. Anal. Chim. Acta 351 (1997) 247
18. T.A. Cool, K. Nakajima, unpublished [The Experimental Conditions are Described, in: T.A. Cool, J. Wang, K. Nakajima, C.A. Taatjes, A. McIlroy, Int. J. Mass Spectrom. 247 (2005) 18].