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Volumn 46, Issue 28, 2007, Pages 5431-5434

Isolation of a cubane-type metal sulfido cluster with a molecular nitrogen ligand

Author keywords

Cluster compounds; Iridium; Nitrogen fixation; Ruthenium; Sulfur

Indexed keywords

CLUSTER COMPOUNDS; CLUSTER CORES; DINITROGEN LIGANDS; SINGLE-CRYSTAL X-RAY ANALYSIS;

EID: 34447570826     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200701044     Document Type: Article
Times cited : (43)

References (38)
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    • Eds, J. A. McCleverty, T. J. Meyer, Elsevier, Amsterdam
    • b) P. L. Holland, Comprehensive Coordination Chemistry II, Vol. 8 (Eds.: J. A. McCleverty, T. J. Meyer), Elsevier, Amsterdam, 2004, p. 569;
    • (2004) Comprehensive Coordination Chemistry II , vol.8 , pp. 569
    • Holland, P.L.1
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    • Ed, F. A. Devillanova, RSC, Cambridge
    • d) Y. Mizobe, Handbook of Chalcogen Chemistry (Ed.: F. A. Devillanova), RSC, Cambridge, 2007, p. 725.
    • (2007) Handbook of Chalcogen Chemistry , pp. 725
    • Mizobe, Y.1
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    • 34447522505 scopus 로고    scopus 로고
    • X-ray data for 2: Mr, 1345.88, 0.25 x 0.20 x 0.12 mm3, triclinic, space group P1, a, 11.458(2, b, 20.407(3, c, 20.800(3) Å, α, 114.068(2, β, 97.869(1, γ, 94.524(1)°, V, 4350(1) Å3, Z, 4, ρcalcd, 2.055 g cm-3, R1 =0.0404 (12 935 data with I > 2σ(I, and wR2, 0.130 (all 19 101 unique data) for 933 variables, GOF, 1.035. 3·CH 2Cl2: Mr, 1720.74, 0.27 x 0.11 x 0.11 mm3, monoclinic, space group P21/c, a, 12.912(2, b, 24.451(3, c, 16.925(2) Å, β, 91.3270(8)°, V, 5342(1) Å3, Z, 4, ρcalcd, 2.140 g cm-3, R1, 0.0380 (7235 data with I > 2σ(I, and wR2, 0.124 all 121 851 unique d
    • -3, R1= 0.0443 (6974 data with I > 2σ(I)) and wR2 = 0.127 (all 10 462 unique data) for 505 variables, GOF = 1.033. CCDC-633248, -633249, -639460, and -633251 (2, 3, 4, and 5, respectively) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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    • 33750494325 scopus 로고    scopus 로고
    • 2 bond: K. Yoshizawa, N. Kihara, Y. Shiota, H. Seino, Y. Mizobe, Bull. Chem. Soc. Jpn. 2006, 79, 53.
    • 2 bond: K. Yoshizawa, N. Kihara, Y. Shiota, H. Seino, Y. Mizobe, Bull. Chem. Soc. Jpn. 2006, 79, 53.
  • 36
    • 34447558965 scopus 로고    scopus 로고
    • CrystalStructure 3.8.0: Crystal Structure Analysis Package, Rigaku and Rigaku/MSC, 2000-2006. CRYSTALS Issue 10: D. J. Watkin, C. K. Prout, J. R. Carruthers, P. W. Betteridge, Chemical Crystallography Laboratory, Oxford, UK.
    • CrystalStructure 3.8.0: Crystal Structure Analysis Package, Rigaku and Rigaku/MSC, 2000-2006. CRYSTALS Issue 10: D. J. Watkin, C. K. Prout, J. R. Carruthers, P. W. Betteridge, Chemical Crystallography Laboratory, Oxford, UK.
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    • PATTY: P. T. Beurskens, G. Admiraal, G. Beurskens, W. P. Bosman, S. Garcia-Granda, R. O. Gould, J. M. M. Smits, C. Smykall, The DIRDIF program system, Technical Report of the Crystallography Laboratory, University of Nijmegen, The Netherlands, 1992.
    • PATTY: P. T. Beurskens, G. Admiraal, G. Beurskens, W. P. Bosman, S. Garcia-Granda, R. O. Gould, J. M. M. Smits, C. Smykall, The DIRDIF program system, Technical Report of the Crystallography Laboratory, University of Nijmegen, The Netherlands, 1992.
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    • DIRDIF99: P. T. Beurskens, G. Admiraal, G. Beurskens, W. P. Bosman, R. de Gelder, R. Israel, J. M. M. Smits, The DIRDIF-99 program system; Technical Report of the Crystallography Laboratory: University of Nijmegen, The Netherlands, 1999.
    • DIRDIF99: P. T. Beurskens, G. Admiraal, G. Beurskens, W. P. Bosman, R. de Gelder, R. Israel, J. M. M. Smits, The DIRDIF-99 program system; Technical Report of the Crystallography Laboratory: University of Nijmegen, The Netherlands, 1999.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.