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The Merck Index
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33749550388
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34447527816
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-1.
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-1.
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34447519239
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Selected Analytical Data 1-Bromo-2-phenylpropan-2-ol 1H NMR (CDCl3, δ, 1.68 (s, 3 H, 2.63 (s, 1 H, 3.73 (dd, 2 H, J1, 12.45 Hz, J2, 10.20 Hz, 7.25-7.49 (m, 5 H) ppm. 13C NMR (CDCl3, δ, 28.0, 46.2, 73.1, 124.8, 127.5, 128.4, 144.2 ppm. MS (70 eV, m/z, 216 [M, 2, 214 [M, 199, 201, 121 (100, 77, 43, 2-Bromo-1- methoxyethyl)benzene 1H NMR (CDCl3, δ, 3.31 (s, 3 H, 3.42-3.59 (m, 2 H, 4.39 (dd, 1 H, J1, 7.86 Hz, J2, 4.44 Hz, 7.34-7.43 (m, 5 H) ppm. 13C NMR (CDCl3, δ, 36.2, 57.2, 83.4, 126.7, 128.6, 139.0 ppm. MS (70 eV, m/z, 216 [M, 2, 214 [M, 121 (100, 91, 77, 51, 2-Bromo-1-isopropoxyethyl)benzene 1H NMR (CDCl 3, δ, 1.12 (d, 3 H, J, 6.15 Hz, 1.23 d, 3 H, J
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+], 99, 81 (100), 57, 41.
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22
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34447500622
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+], 173, 171, 145, 143, 119, 117, 84, 63, 49 ppm.
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+], 173, 171, 145, 143, 119, 117, 84, 63, 49 ppm.
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23
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34447508367
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4-Bromo-N-methylacetanilide Mp 91°C (lit. 13 95°C, 1H NMR (CDCl3, δ, 1.83 (s, 3 H, 3.20 (s, 3 H, 7.04, d, J, 8.30 Hz, 2 H, 7.50 (d, J, 8.30 Hz, 2 H, 13C NMR (CDCl3, δ, 22.4, 37.0, 121.4, 128.7, 132.9, 143.5, 205.6. MS (70 eV, m/z, 229 [M, 2, 227 [M, 187 (100, 185 (100, 186, 184, 157, 155, 104, 77, 56, 43. 4-Bromoacetanilide Mp 166°C (lit.14 167°C, 1H NMR (DMSO-d6, δ, 2.03 (s, 3 H, 7.43, d, J, 8.92 Hz, 2 H, 7.54 (d, J, 8.92 Hz, 2 H) ppm. 13C NMR (DMSO-d6, δ, 24.0, 114.5, 120.8, 131.5, 138.7, 168.5 ppm. MS (70 eV, m/z, 215 [M, 2, 213 [M, 173 (100, 171 (100, 157, 155, 92, 43. 1-Bromo-2- methoxynaphthalene Mp 82°C (lit.15 85°C, 1H NMR CD
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+], 223, 221, 195 (100), 193 (100), 127, 114.
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25
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0141740747
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Yamasaki, R.; Tanatani, A.; Azumaya, I.; Saito, S.; Yamagushi, K.; Kagechika, H. Org. Lett. 2003, 5, 1265.
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Org. Lett
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Yamasaki, R.1
Tanatani, A.2
Azumaya, I.3
Saito, S.4
Yamagushi, K.5
Kagechika, H.6
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26
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77957128027
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Miyano, S.1
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Hashimoto, H.5
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