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Volumn , Issue 11, 2007, Pages 1687-1690

Efficient electrophilic cobromination of alkenes and bromination of activated arenes with bromodichloroisocyanuric acid under mild conditions

Author keywords

Alkenes; Arenes; Electrophilic addition; Electrophilic aromatic substitution; Halogenation

Indexed keywords

1 BROMO 2 METHOXYNAPHTHALENE; 2 METHOXYNAPHTHALENE; ACETANILIDE; ACETIC ACID; ALCOHOL; ALKENE DERIVATIVE; ANISOLE; BROMODICHLOROISOCYANURIC ACID; CYANURIC ACID; MONOBROMOARENE; N METHYLACETANILIDE; NAPHTHALENE DERIVATIVE; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE; REAGENT; UNCLASSIFIED DRUG; WATER;

EID: 34447560067     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-2007-982575     Document Type: Article
Times cited : (43)

References (26)
  • 7
    • 0043126286 scopus 로고    scopus 로고
    • 13rd ed; Merck & Co. Inc, Whitehouse Station
    • The Merck Index, 13rd ed; Merck & Co. Inc.: Whitehouse Station, 2001.
    • (2001) The Merck Index
  • 20
    • 34447527816 scopus 로고    scopus 로고
    • -1.
    • -1.
  • 21
    • 34447519239 scopus 로고    scopus 로고
    • Selected Analytical Data 1-Bromo-2-phenylpropan-2-ol 1H NMR (CDCl3, δ, 1.68 (s, 3 H, 2.63 (s, 1 H, 3.73 (dd, 2 H, J1, 12.45 Hz, J2, 10.20 Hz, 7.25-7.49 (m, 5 H) ppm. 13C NMR (CDCl3, δ, 28.0, 46.2, 73.1, 124.8, 127.5, 128.4, 144.2 ppm. MS (70 eV, m/z, 216 [M, 2, 214 [M, 199, 201, 121 (100, 77, 43, 2-Bromo-1- methoxyethyl)benzene 1H NMR (CDCl3, δ, 3.31 (s, 3 H, 3.42-3.59 (m, 2 H, 4.39 (dd, 1 H, J1, 7.86 Hz, J2, 4.44 Hz, 7.34-7.43 (m, 5 H) ppm. 13C NMR (CDCl3, δ, 36.2, 57.2, 83.4, 126.7, 128.6, 139.0 ppm. MS (70 eV, m/z, 216 [M, 2, 214 [M, 121 (100, 91, 77, 51, 2-Bromo-1-isopropoxyethyl)benzene 1H NMR (CDCl 3, δ, 1.12 (d, 3 H, J, 6.15 Hz, 1.23 d, 3 H, J
    • +], 99, 81 (100), 57, 41.
  • 22
    • 34447500622 scopus 로고    scopus 로고
    • +], 173, 171, 145, 143, 119, 117, 84, 63, 49 ppm.
    • +], 173, 171, 145, 143, 119, 117, 84, 63, 49 ppm.
  • 23
    • 34447508367 scopus 로고    scopus 로고
    • 4-Bromo-N-methylacetanilide Mp 91°C (lit. 13 95°C, 1H NMR (CDCl3, δ, 1.83 (s, 3 H, 3.20 (s, 3 H, 7.04, d, J, 8.30 Hz, 2 H, 7.50 (d, J, 8.30 Hz, 2 H, 13C NMR (CDCl3, δ, 22.4, 37.0, 121.4, 128.7, 132.9, 143.5, 205.6. MS (70 eV, m/z, 229 [M, 2, 227 [M, 187 (100, 185 (100, 186, 184, 157, 155, 104, 77, 56, 43. 4-Bromoacetanilide Mp 166°C (lit.14 167°C, 1H NMR (DMSO-d6, δ, 2.03 (s, 3 H, 7.43, d, J, 8.92 Hz, 2 H, 7.54 (d, J, 8.92 Hz, 2 H) ppm. 13C NMR (DMSO-d6, δ, 24.0, 114.5, 120.8, 131.5, 138.7, 168.5 ppm. MS (70 eV, m/z, 215 [M, 2, 213 [M, 173 (100, 171 (100, 157, 155, 92, 43. 1-Bromo-2- methoxynaphthalene Mp 82°C (lit.15 85°C, 1H NMR CD
    • +], 223, 221, 195 (100), 193 (100), 127, 114.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.