Microwave assisted extraction of drugs of abuse from human urine

Journal of Applied Toxicology

Volumn 27, Issue 4, 2007, Pages 373-379

  Fernández, Purificación ^a   Lago, Marta ^a   Lorenzo, Rosa Antonia ^b   Carro, Antonia María ^b   Bermejo, Ana María ^a   Tabernero, María Jesús ^a  

^a UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

^b UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

Author keywords

Drugs of abuse; Gradient; HPLC DAD; MAE; Urine

Indexed keywords

2 ETHYLIDENE 1,5 DIMETHYL 3,3 DIPHENYLPYRROLIDINE; ACETONITRILE; BENZOYLECGONINE; CHLOROFORM; COCAINE; CODEINE; DICHLOROMETHANE; HOMOCOCAINE; ILLICIT DRUG; METHADONE; MORPHINE; MORPHINE 6 ACETATE; PHOSPHATE; PYRROLIDINE DERIVATIVE; SOLVENT; UNCLASSIFIED DRUG;

ACCURACY; ACIDITY; ARTICLE; DIODE; DIODE ARRAY DETECTOR; EXTRACTION; FACTORIAL DESIGN; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; MICROWAVE ASSISTED EXTRACTION; MICROWAVE IRRADIATION; PRIORITY JOURNAL; SPAIN; URINALYSIS;

CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; COCAINE; CODEINE; HUMANS; HYDROGEN-ION CONCENTRATION; METHADONE; MICROWAVES; MORPHINE; PYRROLIDINES; REPRODUCIBILITY OF RESULTS; SOLID PHASE EXTRACTION; SPECTROPHOTOMETRY, ATOMIC; STREET DRUGS; TIME FACTORS;

EID: 34447539737     PISSN: 0260437X     EISSN: 10991263     Source Type: Journal    
DOI: 10.1002/jat.1216     Document Type: Article

References (25)

1. Antollini L, Suriano C, Grassi MC, Nencini P. 2001. Analysis of cocaethylene, benzoylecgonine and cocaine in human urine by high performance thin layer chromatography with ultraviolet detection: a comparison with high performance liquid chromatography. J. Chromatogr. B 751: 19-27.
2. Brachet A, Christen P, Veuthey JL. 2002. Focused microwave assisted extraction of cocaine and benzoylecgonine from coca leaves. Phytochem. Anal. 13: 162-169.
3. Bresolle F, Bromet-Petit M, Audran M. 1996. Validation of liquid chromatographic and gas chromatographic methods. Applications to pharmacokinetics. J. Chromatogr. 686: 3-10.
4. Brunetto MR, Delgado Cayama Y, Gutiérrez García L, Gallignani M, Obando MA. 2005. Determination of cocaine and benzoylecgonine by direct injection of human urine into a column switching liquid chromatography system with diode array detection. J. Pharm. Biomed. Anal. 37: 115-120.
5. Cardenas S, Gallego M, Valcarcel M. 1996. An automated preconcentration-derivatization system for the determination of cocaine and its metabolites in urine and illicit cocaine samples by gas chromatography/mass spectrometry. Rapid Commun. Mass Spectrom. 10: 631-636.
6. Concheiro M, de Castro A, Quintela O, López-Rivadulla M, Cruz A. 2006. Determination of drugs of abuse and their metabolites in human plasma by liquid chromatography-mass spectrometry. An application to 156 road-fatalities. J. Chromatogr. B 832: 81-89.
7. Cone EJ, Hillsgrove M, Darwin WD. 1994. Simultaneous measurement of cocaine, cocaethylene, their metabolites, and crack pyrolysis products by gas chromatography-mass spectrometry. Clin. Chem. 40: 1299-1305.
8. Cone EJ, Lange R, Darwin WD. 1998. In vivo adulteration: excess fluid ingestion causes false-negative marijuana and cocaine urine test results. J. Anal. Toxicol. 22: 460-473.
9. Croteau LG, Akhtar MH, Bélanger JMR, Paré JRJ. 1994. High performance liquid chromatography determination following microwave assisted extraction of 3-nitro-4-hydroxyphenylarsonic acid from swine liver, kidney and muscle. J. Liquid Chromatogr. 17: 2971-2981.
10. Dams R, Benijts T, Lambert W, De Leenheer AP. 2002. Simultaneous determination of in total 17 opium alkaloids and opioids in blood and urine by fast liquid chromatography diode array detection fluorescence detection, after solid-phase extraction. J. Chromatogr. B 733: 53-61.
11. Elliott SP, Hale KA. 1998. Applications of an HPLC-DAD drugs screening system based on retention indices and UV spectra. J. Anal. Toxicol. 22: 279-289.
12. Eskilsson CS, Björklund E, Mathiasson L, Karlsson L, Tortensson A. 1999. Microwave assisted extraction of felodipine tablets. J. Chromatogr. A 840: 59-70.
13. Foulon C, Menet MC, Manuel N, Pham-huy C, Galons H, Claude JR, Guyon F. 1999. Rapid analysis of benzoylecgonine, cocaine and cocaethylene in urine, serum and saliva by isocratic high performance liquid chromatography with diode array detection. Chromatographia 50: 721-727.
14. Franke M, Winek CL, Kingston HM. 1996. Extraction of selected drugs from serum using microwave irradiation. Forensic Sci. Int. 81: 51-59.
15. Ganzler K, Salgó A, Valkó K. 1986. Microwave extraction. A novel sample preparation method for chromatography. J. Chromatogr. 371: 299-306.
16. Lewis GA, Mathieu D, Phan-Tan-Luu R. 1999. Pharmaceutical Experimental Design. Marcel Dekker: New York.
17. Maraliková B, Weinmann W. 2004. Confirmatory analysis for drugs of abuse in plasma and urine by high performance liquid chromatography tandem mass spectrometry with respect to criteria for compound identification. J. Chromatogr. B 811: 21-30.
18. McCambly K, Kelly RC, Johnson T, Johnson JE, Brown WC. 1997. Robotic solid-phase extraction of amphetamines from urine for analysis by gas chromatography-mass spectrometry. J. Anal. Toxicol. 21: 438-444.
19. Miller JN, Miller JC. 2002. Statistics and Chemometrics for Analytical Chemistry. Prentice Hall: Harlow.
20. Pare JRJ, Belanger JMR. 1994. Microwave assisted process (MAP): a new tool for the analytical laboratory. Trends Anal. Chem. 13: 176-184.
21. Peters FT, Maurer HH. 2002. Bioanalytical method validation and its implications for forensic and clinical toxicology - A review. Accred. Qual. Assur. 7: 441-449.
22. Schanzle G, Li S, Mikus G, Hofmann U. 1999. Rapid, highly sensitive method for the determination of morphine and its metabolites in body fluids by liquid chromatography mass spectrometry. J. Chromatogr. B 721: 55-65.
23. Schramm W, Craig PA, Smith RH, Berger GE. 1993. Cocaine and benzoylecgonine in saliva, serum and urine. Clin. Chem. 39: 481-487.
24. Shah VP, Midha KK, Findlay JW, Hill HM, Hulse JD, McGilveray IJ, Miller KJ, Patnaik RN, Powell ML, Tonelli A, Viswanathan CT, Yacobi A. 2000. Bioanalytical method validation - a revisit with a decade of progress. Pharm. Res. 17: 1551-1557.
25. Williams RH, Maggiore JA, Shah SM, Erickson TB, Negrusz A. 2000. Cocaine and its major metabolite in plasma and urine samples from patients in an emergency medicine setting. J. Anal. Toxicol. 24: 478-482.