Determination of calycosin-7-O-β-D-glucopyranoside in rat plasma and urine by HPLC

Biomedical Chromatography

Volumn 21, Issue 7, 2007, Pages 762-767

  Ye, Guan ^a   Ma, Rong Rong ^b   Li, Zhi Xiong ^a   Wang, Hui ^a   Zhu, Hai Yan ^a   Sun, Zhao Lin ^a   Huang, Cheng Gang ^a  

^a SHANGHAI INSTITUTE OF MATERIA MEDICA   (China)

^b HARBIN UNIVERSITY OF COMMERCE   (China)

Author keywords

Calycosin 7 O D glucopyranoside; HPLC; Plasma; SPE; Urine

Indexed keywords

BODY FLUIDS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PHASE SEPARATION;

CALYCOSIN-7-O-Β-D-GLUCOPYRANOSIDE; GLUCOPYRANOSIDE; HIGH-PERFORMANCE LIQUID CHROMATOGRAPHIC; INTERNAL STANDARDS; LIQUID CHROMATOGRAPHIC ASSAY; PERFORMANCE; RAT PLASMA AND URINES; REVERSED-PHASE HIGH PERFORMANCE; SOLID-PHASE EXTRACTION; URINE;

RATS;

ACETONITRILE; CALYCOSIN 7 O BETA DEXTRO GLUCOPYRANOSIDE; ISOFLAVONOID; RUTOSIDE; UNCLASSIFIED DRUG;

ACCURACY; ANIMAL EXPERIMENT; AREA UNDER THE CURVE; ARTICLE; CONTROLLED STUDY; DRUG BLOOD LEVEL; DRUG CLEARANCE; DRUG DETERMINATION; DRUG EXCRETION; DRUG HALF LIFE; DRUG URINE LEVEL; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MALE; MAXIMUM PLASMA CONCENTRATION; NONHUMAN; RAT; SOLID PHASE EXTRACTION; SPRAGUE DAWLEY RAT; TIME TO MAXIMUM PLASMA CONCENTRATION; VALIDATION PROCESS;

RATTUS;

EID: 34447536131     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.819     Document Type: Article

References (15)

1. Hirotani M, Zhou Y, Lui H and Furuya T. Cycloartane triterpene glycosides from the hairy root cultures of Astragalus membranaceus. Phytochemistry 1994; 37(5): 1403-1407.
2. Huang CG, Zhang YY, Zhu HY, Ma CH, Ye G, Fan MS, Tang YH, Li ZX and Sun ZL. An anti-coxsackie virus isoflavone. Patent No: CN1813711, 2006.
3. Kim EJ and Yang KS. Effect of Astragali Radix on low density lipoprotein oxidation. Yakhak Hoechi 2001; 45(5): 529-535.
4. Kim EJ, Jin OO, Lee SK and Yang KS. Inhibitory effect of astragali radix on COX-2 activity. Saengyak Hakhoechi 2001; 32(4): 311-315.
5. Lin LZ, He XG, Lindenmaier M, Nolan G and Yang J. Liquid chromatography-electrospray ionization mass spectrometry study of the flavonoids of the roots of Astragalus mongholicus and membranaceus. Journal of Chromatography A 2000; 876(1-2): 87-95.
6. Rios JL and Waterman PG. A review of the pharmacology and toxicology of Astragalus. Phytotherapy Research 1997; 11(6): 411-418.
7. Shimizu N, Tomoda M, Kanari M and Gonda R. An acidic polysaccharide having activity on the reticuloendothelial system from the root of Astragalus mongholicus. Chemical and Pharmaceutical Bulletin 1991; 39(11): 2969-2972.
8. Subarnas A, Oshima Y and Hikino H. Isoflavans and a pterocarpan from Astragalus mongholicus. Phytochemistry 1991; 30(8): 2777-2780.
9. Tomoda M, Shimizu N, Ohara N, Gonda R, Ishii S and Otsuki H. A reticuloendothelial system-activating glycan from the roots of Astragalus membranaceus. Phytochemistry 1992; 31(1): 63-66.
10. Wu DZ, Hu ZB, Zhou JY and Fan Y. Calycosin and calycosin-7-O-beta-glucoside of Astragalus membrannaceus, which have the inhibitory effect on myocardial ischemia. CN1403452, 2003.
11. Wu T, Annie Bligh SW, Gu LH, Wang ZT, Liu HP, Cheng XM, Branford-White CJ and Hu ZB. Simultaneous determination of 6 isoflavonoids in commercial Radix Astragali by HPLC-UV. Fitoterapia 2005; 76(2): 157-165.
12. Xiao HB, Krucker M, Albert K and Liang XM, Determination and identification of isoflavonoids in Radix astragali by matrix solid-phase dispersion extraction and high-performance liquid chromatography with photodiode array and mass spectrometric detection. Journal of Chromatography A 2004; 1032(1-2): 117-124.
13. Xie ZF, Lou ZC and Huang XK. Classified Dictionary of Traditional Chinese Medicine. New World Press: Beijing, 1994; 374.
14. Yu DH, Duan YL, Bao YM, Wei CL and An LJ. Isoflavonoids from Astragalus mongholicus protect PC12 cells from toxicity induced by L-glutamate. Journal of Ethnopharmacology 2005; 98(1-2): 89-94.
15. Zheng ZR, Song CQ, Liu T and Hu ZB. Determination of six isoflavonoids in the root cultures of Astragalus membranaceus by HPLC. Yaoxue Xuebao 1998; 33(2): 148-151.