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Volumn 46, Issue 13, 2007, Pages 5134-5136

Ferromagnetic vs antiferromagnetic coupling in bis(μ-phenoxo) dicopper(II) complexes. Tuning of the nature of exchange coupling by remote ligand substituents

(3) Chaudhuri, Phalguni a Wagner, Rita a Weyhermüller, Thomas a

a MAX PLANCK INSTITUTE FOR CHEMICAL ENERGY CONVERSION (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

COPPER; DIPHENYL ETHER DERIVATIVE; FERRIC ION; FERRITE; LIGAND; ORGANOMETALLIC COMPOUND;

ARTICLE; CHEMISTRY; MAGNETISM;

COPPER; FERRIC COMPOUNDS; LIGANDS; MAGNETICS; ORGANOMETALLIC COMPOUNDS; PHENYL ETHERS;

EID: 34447344856 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic070238p Document Type: Article

Times cited : (53)

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19
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- Complex 1: To the pale-yellow solution containing H 2LCH3 (0.3 g, 1 mmol) and Et3N (0.5 mL) in dry acetonitrile (50 mL) was added [CuI(CH3CN) 4]ClO4 (0.33 g, l mmol, and the solution was refluxed under argon for 0.5 h, upon which the solution turned to red-brown with a copper mirror on the surface of the round-bottomed flask. The solution was cooled and brought to air with stirring for 0.5 h. The precipitated dark-green microcrystalline solid was isolated by filtration and air-dried. Yield: 0.14 g (39, Anal. Calcd for C38H46N2O 4Cu2: C, 63.22; H, 6.42; N, 3.88; Cu, 17.61. Found: C, 62.9; H, 6.4; N, 3.9; Cu, 18.0. MS-EI: m/z 721 (M, 360 (M+/2, UV-vis in CH2Cl2 (λ, nm; ε, M-1 cm-1, 423 (5600, 620 (8200, 760sh (∼350, IR KBr, cm-1, 2914, 1634
- -1): 2959, 2904, 2868, 2678, 1604, 1474, 1442, 1413, 1360, 1305, 1284, 1236, 1166, 1095, 836, 827.

20
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- Crystal data for 1: C38H46Cu 2N2O4·CH3CN·0.5H 2O, Mf, 771.91, T, 100(2) K, triclinic, a, 11.6777(9) Å, b, 12.908(2) Å, c, 13.519-(2) Å, α, 79.69(2)°, β, 77.03(2)°, γ, 67.96(2)°, V, 1830.3(4) Å3, space group P1, Z, 2. A total of 5111 independent reflections was used for solution and refinement (SHELX97) by full-matrix least squares on F 2; absorption correction, Gaussian, face-indexed. Final R indices: R1, 0.0522, R1(all data, 0.0855. Crystal data for 2: C 62H94Cu2N2O4, Mf, 1058.47, T, 100(2) K, triclinic, a, 10.0842-(6) Å, b, 10.7271(6) Å, c, 27.6144(14, α, 93.97(1)°, β, 94.92
- 2. Final R indices: R1 = 0.0351. R1(all data) = 0.0417.

21
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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.