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The crystal data for 2 were collected on a Bruker X8 APEX diffractometer with a CCD area detector and multilayer mirror monochromated MoKα radiation. The structure was solved using direct methods, refined with the Shelx software package (G. Sheldrick, Universität Göttingen, 1997, and expanded using Fourier techniques. All non-hydrogen atoms were refined anisotropically. Hydrogen atoms were assigned idealized positions and were included in structure-factor calculations. Crystal data for 2: C20H33BFeO 2Si2, Mr, 428.30, yellow block, 0.18 x 0.12 x 0.05 mm3, triclinic, space group P1, a, 7.0700(3, b, 9.8671 (4, c, 17.4633(7) Å, α, 86.591(2, β, 81.624(2, γ, 84.886(2)°, V, 1199.12(9) Å3, Z, 2, ρcalcd, 1.186 g cm -3, μ, 0.739 m
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2 = 0.1678, 11 075 independent reflections (2θ = 74.34°) and 246 parameters. CCDC-633058 (2) contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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