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Volumn 48, Issue 32, 2007, Pages 5605-5608

Synthesis of monosaccharide units using fluorous method

Author keywords

[No Author keywords available]

Indexed keywords

FLUORINE; MONOSACCHARIDE; ORGANIC SOLVENT;

EID: 34447271948     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2007.06.068     Document Type: Article
Times cited : (17)

References (30)
  • 18
    • 34447273372 scopus 로고    scopus 로고
    • note
    • meso-Erythritol (1) was commercially available (Wako Pure Chemical Industries, Ltd).
  • 20
    • 34447256867 scopus 로고    scopus 로고
    • note
    • +: 1617.6; found, 1617.6.
  • 21
    • 34447260964 scopus 로고    scopus 로고
    • note
    • Per-O-acetyl-β-d-glucopyranose (6) and per-O-acetyl-β-d-galactopyranose (13) were commercially available (TOKYO KASEI KOGYO CO., LTD).
  • 22
    • 34447254777 scopus 로고    scopus 로고
    • note
    • 9 is a commercially available fluorocarbon solvent (3M, Tokyo), which is called Novec™ HFE-7100 and miscible in common organic solvents and fluorous solvents.
  • 23
    • 24044520028 scopus 로고    scopus 로고
    • Yu, M. S.; Curran, D. P.; Nagashima, T. Org. Lett. 2005, 7, 3677. We improved the condition of the partitioning in this reference.
  • 24
    • 34447249806 scopus 로고    scopus 로고
    • note
    • 14) isomers and is called Fluorinert™ FC-72.
  • 25
    • 34447249808 scopus 로고    scopus 로고
    • note
    • 9-FC72 = 4:1) and 95% aq MeCN. Compound 10 was partitioned between fluorous mixed solvent and 95% aq MeOH. Compound 16 was partitioned between FC72 and toluene. None of the fluorous compounds were detected by TLC of the organic layer after three extractions with FC72, which shows that these compounds were quantitatively extracted in the fluorous layer.
  • 26
    • 34447264540 scopus 로고    scopus 로고
    • note
    • +: 2064.1; found, 2063.4.
  • 27
    • 34447249809 scopus 로고    scopus 로고
    • note
    • +: 466.9715; found, 466.9687.
  • 30
    • 34447256866 scopus 로고    scopus 로고
    • note
    • +: 2428.8; found, 2429.7.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.