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34347261847
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2O/acetic acid/pyridine (90:10:0.5:0.5, v/v); three analytical-scale C-18 columns (4.6 × 250 mm; 5 μm silica particle size) connected in series; thermal gradient using column oven (0 min-40°C; 10 min-40°C; 50 min-80°C; 55 min-80°C).
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2O/acetic acid/pyridine (90:10:0.5:0.5, v/v); three analytical-scale C-18 columns (4.6 × 250 mm; 5 μm silica particle size) connected in series; thermal gradient using column oven (0 min-40°C; 10 min-40°C; 50 min-80°C; 55 min-80°C).
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34347232468
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Crystal data for compound 1: C30H30N4OV, Mr, 513.53, monoclinic, space group C2/c, 15, a, 24.904(4, b, 13.7017(17, c, 15.5939(16) Å, β, 113.926(6)°, V, 4863.8(10) Å3, Z, 8, Cu Kα radiation (λ, 1.54187 Å, Dcalcd, 1.403 g cm-3, μ(Cu Kα, 36.580 cm -1, 21674 measured reflections, 4441 unique reflections [R int, 0.109; I > -3σ(I, 4441 reflections included in the refinement, R, 0.108 [1529 reflections with I > 2σ(I, wR, 0.371 (all reflections, Crystallographic data for the structural analysis of compound 1 has been deposited with the Cambridge Crystallographic Data Centre CCDC No. 627948, Copies of this information can be obtained free of charge via, www.ccdc.carn.ac.uk/conts/retrieving.html
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int = 0.109; I > -3σ(I)], 4441 reflections included in the refinement, R = 0.108 [1529 reflections with I > 2σ(I)], wR = 0.371 (all reflections). Crystallographic data for the structural analysis of compound 1 has been deposited with the Cambridge Crystallographic Data Centre (CCDC No. 627948). Copies of this information can be obtained free of charge via, www.ccdc.carn.ac.uk/conts/retrieving.html.
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0022923453
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ed. by R. B. Johns, Elsevier, Netherland
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34347249337
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H. J. Callot, R. Ocampo, in The Porphyrin Handbook, 1, Synthesis and Organic Chemistry, ed. by K. M. Kadish, K. M. Smith, R. Guiland, Academic Press, San Diego, 2000, pp. 349-398.
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b) H. J. Callot, R. Ocampo, in The Porphyrin Handbook, Vol. 1, Synthesis and Organic Chemistry, ed. by K. M. Kadish, K. M. Smith, R. Guiland, Academic Press, San Diego, 2000, pp. 349-398.
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