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22
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0037121867
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O. I. Shchegolikhina, Y. A. Pozdnyakova, Y. A. Molodtsova, S. D. Korkin, S. S. Bukalov, L. A. Leites, K. A. Lyssenko, A. S. Peregudov, N. Auner, D. E. Katsoulis, Inorg. Chem. 2002, 41, 6892.
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23
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34347257551
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All compounds obtained here showed satisfactory spectral data
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All compounds obtained here showed satisfactory spectral data.
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24
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0000780743
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a) M. A. Hossain, M. B. Hursthouse, K. M. A. Malik, Acta Crystallogr., Sect. B1979, 35, 2258.
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25
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0011698390
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b) W. Clegg, G. M. Sheldrick, N. Vater, Acta Crystallogr., Sect. B 1980, 36, 3162.
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Clegg, W.1
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27
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34347248903
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Crystal data at 150K for 2e: C56H56O 12Sig, fw 1145.72, tetragonal, a, 21.3476(22, b, 21.3476(22, c, 12.4353(14)Å, α, 90.000(0)°, β, 90.000(0)°, γ, 90.000(0)°, V, 5667.02(0) Å3, space group: 14/a, Z, 8, Dcalcd, 1.34g-cm-3. For 5f: C28H42O21Si8, fw 1107.82, triclinic, a=11.7860(83, b, 12.4310(63, c= 18.2640(113) Å, α= 96.973(32)°, β= 95.035(25)°, γ, 101.934(28)°, V, 2581.1(28) Å3, space group: PĪ, Z, 2, D calcd, 1.43g·Cm-3. The final R factors were 0.063 and 0.122 (Rw, 0.065 and 0.263 all data) for 3199 and 10939 reflections with I > 2σI, respectively
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w = 0.065 and 0.263 all data) for 3199 and 10939 reflections with I > 2σ(I), respectively.
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