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34347237380
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Crystallographic data of I: C14H16N 2·C10H10O4·2CH 4O, MW 470.56, orthorhombic, space group P212 12, a, 9.4477(10, b, 16.2721(18, c, 7.7928(9) Å, U, 1198.0(2) Å3, Z, 4, D calcd, 1.304g cm-3, μ(Mo Kα, 0.093 mm -1, 7630 reflections measured, 2807 unique, final R (F 2, 0.0468 using 2212 reflections with 1 > 2.0σ(I, Rall data, 0.0682, T, 100 K. CCDC 641519
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2) = 0.0468 using 2212 reflections with 1 > 2.0σ(I), R(all data) = 0.0682, T = 100 K. CCDC 641519.
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19
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34347247414
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Crystallographic data of II: C14H16N 2·C10H10O4·2CH 4O, MW 470.56, orthorhombic, space group P212 12, a, 10.3198(8, b, 15.8863(12, c, 7.7311(6) Å, U, 1267.46(17) Å3, Z, 4, Dcalcd, 1.233g cm-3, μ(Mo Kα, 0.087 mm-1, 7837 reflections measured, 2877 unique, final R (F 2, 0.0294 using 2785 reflections with I > 2.0σ(I, R(all data, 0.0305, T, 100 K. CCDC 641520. Copies of the data can be obtained free of charge via or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk
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2) = 0.0294 using 2785 reflections with I > 2.0σ(I), R(all data) = 0.0305, T = 100 K. CCDC 641520. Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk).
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