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Volumn 633, Issue 8, 2007, Pages 1125-1126

K2[(UO2)As2O7] - The first uranium polyarsenate

Author keywords

Crystal structure; Polyarsenate; Uranium

Indexed keywords

EID: 34250901563 PISSN: 00442313 EISSN: 15213749 Source Type: Journal
DOI: 10.1002/zaac.200700020 Document Type: Article

Times cited : (25)

References (20)

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- Crystallographic data for K2[(UO2)As 2O7, orthorhombic, Pmmn, a, 12.601(2, b, 13.242(2, c, 5.621(1) Å, V, 937.9(3) Å3, Z, 4, ρcalc, 4.320 g/cm 3, 2θmax, 54.20°, λ(Mo κα, 0.71073 Å, φ-scan (Mar345 Image Plate, 293 K, 6767 measured reflections, 1118 independent reflections, 1059 reflections with |Fo| ≥ 4σF (R int, 0.048, Rσ, 0.033, structure solution by direct methods, full-matrix least-square refinement (79 parameters) on |F2, programs SHELXS-97 and SHELXL-97 G.M. Sheldrick, program for the refinement of crystal structures, Göttingen 1997, R1, 0.049, wR2, 0.1060 for observed reflections, R1, 0.052, wR2
- 2 = 0.108 for all data, max/min electron density = 1.936 / -1.771.

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