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+). Caution! Perchlorate salts of metal complexes with organic ligands are potentially explosive and should be handled in small quantities and with care.
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+). Caution! Perchlorate salts of metal complexes with organic ligands are potentially explosive and should be handled in small quantities and with care.
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34250745456
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Crystallographic data for 1: C28H 33ClCuN8O8SZn, M, 806.04 g mol -1, green-brown prism, size 0.5 x 0.5 x 0.4 mm3, monoclinic, space group P21/n, a, 13.1711(3) Å, b, 14.7432(7) Å, c, 17.2400(7) Å, β, 93.042(2)°, V, 3343.0(2) Å3, Z, 4, T, 183(2) K, ρcalcd, 1.602 g cm-3, μ, 1.557 mm-1, 23 395 reflections, 1.90° ≤ θ ≤ 27.48°, 7625 independent reflections, Rint, 0.052, 5499 reflections with I ≥ 2σ(I, 444 parameters, R1, 0.055 (observed, wR2, 0.145 all data, GOF, 1.045. Crystallographic data can be obtained free of charge as CCDC-633833 from the Cambridge Crystallographic Data Centre via, Cambridge CB2 1EZ, U.K
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int = 0.052, 5499 reflections with I ≥ 2σ(I), 444 parameters, R1 = 0.055 (observed), wR2 = 0.145 (all data), GOF = 1.045. Crystallographic data can be obtained free of charge as CCDC-633833 from the Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif or 12 Union Road, Cambridge CB2 1EZ, U.K.
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22
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34250710849
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XSophe Computer Simulation Software Suite, version 1.1.4; Bruker Biospin GmbH: Rheinstetten, Germany, 2004
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XSophe Computer Simulation Software Suite, version 1.1.4; Bruker Biospin GmbH: Rheinstetten, Germany, 2004.
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0037324796
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