One-pot synthesis of 7H-dibenzo[b,d]azepin-7-one by heterogeneous flash vacuum pyrolysis with MCM-41 catalysts

Organic Letters

Volumn 9, Issue 11, 2007, Pages 2179-2181

  Moyano, Elizabeth L ^a   Lucero, Paola L ^a   Eimer, Griselda A ^b   Herrero, Eduardo R ^b   Yranzo, Gloria I ^a  

^a Ciudad Universitaria   (Argentina)

^b Universidad Tecnologica Nacional Facultad Regional COrdoba   (Argentina)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 34250670704     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol070690c     Document Type: Article

References (21)

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8. -2 s with pressures of 0.2 to 0.1 Torr . Products were trapped at the liquid air temperature, extracted with solvent, and submitted to different analyses or separation techniques.
9. In a typical run 0.50 g of fractured catalyst was placed along the reactor (30 cm length, 1 cm diameter) with use of ceramic wool fiber as an inert support. All catalysts were preactivated in air at 500°C for 4 h before each reaction.
10. Prepared by a reported procedure, see: Katritzky. A. R.; Wu, J. Synthesis 1994, 597.
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20. 2/g.
21. Diameter between 1 and 10 nm.