Separation of triacylglycerol species from interesterified oils by high-performance liquid chromatography

JAOCS, Journal of the American Oil Chemists' Society

Volumn 84, Issue 3, 2007, Pages 211-217

  Lee, Jeung Hee ^a   Jones, Kerby C ^b   Foglia, Thomas A ^b   Nuñez, Alberto ^b   Lee, Jong Ho ^c   Kim, Yu Mi ^d   Vu, Phuong Lan ^d   Lee, Ki Teak ^d  

^a UNIVERSITY OF GEORGIA   (United States)

^b EASTERN REGIONAL RESEARCH CENTER   (United States)

^c Yonsei University   (South Korea)

^d Chungnam National University   (South Korea)

Author keywords

APCI mass spectrometry evaporated light scattering detection; Low calorie structured lipids; Reversed phase and normal phase high performance liquid chromatography

Indexed keywords

COLUMN CHROMATOGRAPHY; ENZYME KINETICS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIGHT SCATTERING; LIPASES; MASS SPECTROMETRY; SEPARATION;

LIGHT SCATTERING DETECTION; OLIVE OIL; REVERSED PHASE HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY; SOYBEAN OIL; TRIACYLGLYCEROL;

FATTY ACIDS;

GLYCINE MAX;

EID: 34250617080     PISSN: 0003021X     EISSN: None     Source Type: Journal    
DOI: 10.1007/s11746-006-1029-x     Document Type: Article

References (14)

1. Willis WM, Lencki RW, Marangoni AG (1998) Lipid modification strategies in the production of nutritionally functional fats and oils. Crit Rev Food Sci Nutr 38:639-679
2. Akoh CC (1995) Structured lipids: enzymatic approach. INFORM 6:1055-1061.
3. Iwasaki Y, Yamane T (2000) Enzymatic synthesis of structured lipid. J Mol Catal B 20:129-140
4. Willis WM, Marangoni AG (2002) Enzymatic interesterification. In: Akoh CC, Min DB (eds) Food lipids: chemistry, nutrition and biotechnology, 2nd edn. Marcel Dekker, New York, pp 839-875
5. Klemann LP, Aji K, Chrysam MM, D'Amelia RP, Henderson JM, Huang AS, Otterburn MS, Yarger RG, Boldt G, Roden A (1994) Random nature of triacylglycerols produced by the catalyzed interesterification of short- and long-chain fatty acid triglycerides. J Agric Food Chem 42:442-446
6. Lee JH, Jones KC, Lee KT, Kim MR, Foglia TA (2003) High-performance liquid chromatographic separation of structured lipids produced by interesterification of macadamia oil with tributyrin and tricaprylin. Chromatogr 58:653-658
7. Byrdwell WC (2005) Qualitative and quantitative analysis of triacylglycerols by atmospheric pressure ionization (APCI and ESI) mass spectrometry techniques. In: Byrdwell WC (ed) Modern methods for lipid analysis by liquid chromatography/mass spectrometry and related techniques. AOCS Press, Champaign, pp 298-412
8. Fauconnot L, Hau J, Aeschlimann J-M, Fay L-B, Dionisi F (2004) Quantitative analysis of triacylglycerol regioisomers in fats and oils using reversed phase chromatography and atmospheric pressue chemical ionization mass spectrometry. Rapid Commun Mass Spectrom 18:218-224
9. Lee JH, Kim MR, Kim H, Kim IH, Lee KT (2003) Characterization of lipase-catalyzed structured lipids from selected vegetable oils with conjugated linoleic acid: their oxidation stability with rosemary extracts. J Food Sci 68:1653-1658
10. Fomuso LB, Akoh CC (2002) Lipase-catalyzed acidolysis of olive oil and capric acid in a bench-scale packed bed bioreactor. Food Res Intern 35:15-21
11. Cossignani L, Damiani P, Siminetti SM, Manes J (2004) Biocatalyzed acidolysis of soybean oil triacylglycerols to increase oleic acid content. J Chromatogr A 1052:167-170
12. Ruiz-Gutiérrez V, Barron LJR (1995) Review: methods for the analysis of triacylglycerols. J Chromatogr B 671:133-168
13. Xu X, Fumuso LB, Akoh CC (2000) Synthesis of structured triacylglycerols by lipase-catalyzed acidolysis in a packed bed bioreactor. J Agri Food Chem 48:3-10
14. Torres CF, Munir F, Blanco RM, Otero C, Hill CG Jr (2002) Catalytic traneseterification of corn oil and tristearin using immolibilized lipase form Thermomyces lanuginose. J Am Oil Chem Soc 79:775-781