Application of mixtures of tartaric acid derivatives in resolution via supercritical fluid extraction

Chirality

Volumn 19, Issue 6, 2007, Pages 430-433

  Kmecz, Ildikó ^a   Simándi, Béla ^a   Székely, Edit ^a   Lovász, Judit ^a   Fogassy, Elemér ^a  

^a BUDAPEST UNIVERSITY OF TECHNOLOGY AND ECONOMICS   (Hungary)

Author keywords

Carbon dioxide; Enantiomer separation; Mixture of related structure resolving agents; Nonlinear behavior; Supercritical fluid extraction

Indexed keywords

ACID; CARBON DIOXIDE; METHAMPHETAMINE; O,O' DI 4 TOLUOYLTARTARIC ACID; O,O' DIBENZOYLTARTARIC ACID; SOLVENT; TARTARIC ACID DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CHIRALITY; DIASTEREOISOMER; ENANTIOMER; OPTICAL ROTATION; PRIORITY JOURNAL; SEPARATION TECHNIQUE; SUPERCRITICAL FLUID EXTRACTION;

EID: 34250182703     PISSN: 08990042     EISSN: 1520636X     Source Type: Journal    
DOI: 10.1002/chir.20362     Document Type: Article

References (9)

1. Rouhi AM. Chiral chemistry. Chem Eng News 2004;82:47-62.
2. Vries T, Wynberg H, van Echten E, Koek J, ten Hoeve W, Kellogg RM, Broxterman QB, Minnaard A, Kaptein B, van der Sluis S, Hulshof LA, Kooistra J. The family approach to the resolution of racemates. Angew Chem Int Ed 1998;37:2349-2353.
3. Nieuwenhuijzen JW, Grimbergen RFP, Koopman C, Kellogg RM, Vries TR, Pouwer K, van Echten E, Kaptein B, Hulshof LA, Broxterman QB. The role of nucleation inhibition in optical resolutions with families of resolving agents. Angew Chem Int Ed 2002;41:4281-4286.
4. Dalmolen J, Tiemersma-Wegman TD, Nieuwenhuijzen JW, van der Sluis, van Echten E, Vries TR, Kaptein B, Broxterman QB, Kellog RM. The Dutch resolution variant of the classical resolution of racemates by formation of diastereomeric salts: Family behaviour in nucleation inhibition. Chem Eur J 2005;11:5619-5624.
5. Markovits I, Egri G, Fogassy E. Nonlinearity in optical resolution via distillation applying mixtures of resolving agents. Chirality 2002;14:674-676.
6. Schindler J, Egressy M, Bálint J, Hell Z, Fogassy E. Optical resolution by crystallization from melt using enantiomer derivatives as resolving agents: Nonlinear behavior of resolving agent mixtures. Chirality 2005;17:565-569.
7. Fogassy E, Ács M, Szili T, Simándi B, Sawinsky J. Molecular chiral recognition in supercritical solvents. Tetrahedron Lett 1994;35:257-260.
8. Simándi B, Keszei S, Fogassy E, Sawinsky J. Supercritical fluid extraction: A novel method for production of enantiomers. J Org Chem 1997;62:4390-4394.
9. Kozma D, Simon H, Pokol G, Fogassy E. Enantiomeric enrichment of partially resolved N-methylamphetamine. J Therm Anal Calorim 2002;69:409-416.