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Volumn 36, Issue 5, 2007, Pages 584-585

Aromatic fluorination effect on the mesomorphic properties of discotic liquid crystal of alkoxybenzoyloxytriphenylene

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EID: 34250172037 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2007.584 Document Type: Article

Times cited : (7)

References (12)

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2
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4
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6
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- b) B. Alameddine, O. F. Aebischer, W. Amrein, B. Donnio, R. Deschenaux, D. Guillon, C. Savary, D. Scanu, O. Scheidegger, T. A. Jenny, Chem. Mater. 2005, 17, 4798.
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- Alameddine, B.¹ Aebischer, O.F.² Amrein, W.³ Donnio, B.⁴ Deschenaux, R.⁵ Guillon, D.⁶ Savary, C.⁷ Scanu, D.⁸ Scheidegger, O.⁹ Jenny, T.A.¹⁰

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9
- 34250162967
- C6F4: 1HNMR (CDCl3, TMS, 500.0 MHz) δ 0.96 (t, J, 6.9Hz, 18H, 1.38-1.41 (m, 24H, 1.52 (quintet, J, 7.0Hz, 12H, 1.84 (quintet, J, 6.7Hz, 12H, 4.33 (t, J, 6.5Hz, 12H, 7.97 (s, 6H, 19FNMR (CDCl3, CFCl 3, 470.0 MHz) δ -138.9 (s, 12F, 158.8 (s, 12F, MS m/z, 1981.8 (calcd 1981.7 for C96H84F24O 18, FT-IR (KBr, cm-1) 2959, 2934, 2361, 2861, 2342, 1759, 1650, 1489, 1412, 1389, 1323, 1256, 1210, 1117, 1006, 939, 890, 835, 800; Anal. Calcd for C96H84F24O18: C, 58.19; H, 4.27; F, 23.01, Found: C, 58.29; H, 4.29; F, 23.11
- 18: C, 58.19; H, 4.27; F, 23.01%. Found: C, 58.29; H, 4.29; F, 23.11%.

10
- 34250221590
- C10F4: 1HNMR (CDCl3, TMS, 500.0MHz) δ 0.91 (t, J, 6.5 Hz, 18H, 1.31-1.40 (m, 72H, 1.51 (quintet, J, 7.5 Hz, 12H, 1.84 (quintet, J, 7.0 Hz, 12H, 4.34 (t, J, 6.5Hz, 12H, 8.07 (s, 6H, 19F NMR (CDCl3, CFCl3, 470.0 MHz, δ -138.8 (s, 12F, 158.4 (s, 12F, MS m/z, 2318.0 (calcd 2318.3 for C120H132F 24O18, FT-IR (KBr, cm-1) 2951, 2926, 2861, 2361, 2342, 1759, 1650, 1489, 1412, 1389, 1323, 1256, 1210, 1117, 1006, 939, 890, 835, 800; Anal. Calcd for C120H132F 24O18: C, 62.17; H, 5.74; F, 19.67, Found: C, 62.22; H, 5.69; F, 19.77
- 18: C, 62.17; H, 5.74; F, 19.67%. Found: C, 62.22; H, 5.69; F, 19.77%.

11
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12
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