Hydrothermal synthesis, characterization and magnetic properties of a new 2D arsenic-vanadate layers supported cobalt coordination complex: [Co(en)2(H2O)]{[Co(en)2]2As8V14O42(SO4)} · 3H2O

Inorganic Chemistry Communications

Volumn 10, Issue 7, 2007, Pages 849-852

  Zhou, Guangpeng ^a   Xu, Yan ^a   Guo, Chunyan ^a   Zheng, Xuefang ^b  

^a LIAONING NORMAL UNIVERSITY   (China)

^b DALIAN UNIVERSITY   (China)

Author keywords

Arsenic vanadate; Cluster; Crystal structure; Hydrothermal synthesis

Indexed keywords

EID: 34249872712     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2007.04.009     Document Type: Article

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41. 2 = 0.1014. The single crystal of the compound 1 was chosen onto a thin glass fiber by epoxy glue in air for data collection. And the diffraction data were collected on a Bruker Apex2 CCD with Mo Kα radiation (λ = 0.71073 Å) at 293 K using ω-2θ scan method. An empirical absorption correction was applied. All of the non-hydrogen atoms were refined anisotropically, while the hydrogen atoms of organic molecule for compound 1 were refined in calculated positions, assigned isotropic thermal parameters, and allowed to ride their parent atoms. All calculations were performed using the SHELX97 program package.
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