Synthesis of cement based CaO-Al2O3-SiO2-H2O (CASH) hydroceramics at 200 and 250 °C: Ex-situ and in-situ diffraction

Cement and Concrete Research

Volumn 37, Issue 6, 2007, Pages 823-833

  Meller, Nicola ^a   Hall, Christopher ^a   Kyritsis, Konstantinos ^a   Giriat, Gaetan ^a  

^a UNIVERSITY OF EDINBURGH   (United Kingdom)

Author keywords

Hydration; Hydroceramics; Kinetics; Oil well cement; X ray diffraction

Indexed keywords

ALUMINA; GEOTHERMAL WELLS; HYDROTHERMAL SYNTHESIS; PHASE COMPOSITION; SILICA; X RAY DIFFRACTION ANALYSIS;

AUTOCLAVED CONSTRUCTION MATERIALS; HYDROCERAMIC COMPOSITIONS; OIL WELL CEMENT;

CHLORINE COMPOUNDS;

EID: 34249302439     PISSN: 00088846     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cemconres.2007.03.006     Document Type: Article

References (35)

1. Carter G., and Smith D.K. Properties of cementing compositions at elevated temperatures and pressure. Trans. Metall. Soc. AIME 213 (1958) 20-27
2. Nelson E. Well Cementing (1990), Schlumberger Educational Services, Sugar Land, Texas
3. Taylor H.F.W. The calcium silicate hydrates. In: Taylor H.F.W. (Ed). The Chemistry of Cements (1964), Academic Press, London 168-232
4. V. Barlet-Gouédard, S. Danican, E. Nelson, C. Cambus, Cement compositions for high temperature applications, PCT Patent Application WO 03/068708, 21 August 2003.
5. V. Barlet-Gouédard, B. Goffé, Cementing compositions and application of these compositions to cementing oil wells or the like, PCT Patent Application WO 01/70646, 27 September 2001.
6. Barlet-Gouédard V., and Vidick B. A non-conventional way of developing cement slurry for geothermal wells. Geotherm. Res. Counc. Trans. 25 (2001) 85-91
7. Meller N., and Hall C. Hydroceramic sealants for geothermal wells. In: Pecchio M., Andrade F.R.D., D'Agostino L.Z.D., Kahn H., Sant'Agostigno L.M., and Tassinari M.M.M.L. (Eds). International Congress on Applied Mineralogy, Internation Council for Applied Mineralogy do Brasil (2004) 281-284
8. 2O hydroceramic system at 200 °C. Mater. Res. Bull. 40 (2005) 715-723
9. Hall C., and Scrivener K.L. Oilwell cement clinkers-X-ray microanalysis and phase composition. Adv. Cem. Based Mater. 7 (1998) 28-38
10. Nelson E., and Eilers L.H. Cementing steamflood and fireflood wells-slurry design. J. Can. Pet. Technol. 25 5 (1985) 58-63
11. Scrivener K.L., Fullmann T., Gallucci E., Walenta G., and Bermejo E. Quantitative study of Portland cement hydration by X-ray diffraction/Rietveld analysis and independent methods. Cem. Concr. Res. 34 (2004) 1541-1547
12. Fletcher D.A., McMeeking R.F., and Parkin D. The United Kingdom chemical database service. J. Chem. Inf. Model. 36 (1996) 746-749
13. Barnes P., Colston S.L., Jupe A.C., Jacques S.D.M., Attfield M., Pisula R., Morgan S., Hall C., Livesey P., and Lunt S. The use of synchrotron sources in the study of cement materials. In: Bensted J., and Barnes P. (Eds). Structure and Performance of Cements (2002), Spon Press, London
14. N. Meller, C. Hall, K. Kyritsis, G. Giriat, H. J. Jakobsen, J. Skibsted, Incorporation of aluminium guest ions in nominally alumina-free calcium silicate hydrates: effects on crystal structure and thermal stability, in Proceedings of the 12th International Congress on the Chemistry of Cement, Montreal, July 2007.
15. Yanagisawa K., Hu X., Onda A., and Kajiyoshi K. Hydration of β-dicalcium silicate at high temperatures under hydrothermal conditions. Cem. Concr. Res. 36 (2006) 810-816
16. Nelson E. Thermal cements. In: Nelson E. (Ed). Well Cementing (1990), Schlumberger Educational Services, Sugar Land, Texas
17. Taylor H.F.W. Cement Chemistry (1997), Thomas Telford Publishing, London
18. Esteban J.J., Cuevas J., and Tubia J.M. Xonotlite in rodingite assemblages from the Ronda Peridotites, Betic Cordilleras, southern Spain. Can. Mineral. 41 (2003) 161-170
19. Merlino S. Gyrolite: its crystal structure and crystal chemistry. Mineral. Mag. 52 (1988) 377-387
20. 2 modification on hydrogarnets formation during hydrothermal synthesis. Cem. Concr. Res. 33 (2003) 1789-1793
21. 2 at temperatures below 90 °C. J. Solid State Chem. 179 (2006) 2988-2997
22. Jupe A.C., Wilkinson A.P., Luke K., and Funkhouser G.P. Class H oil well cement hydration at elevated temperatures in the presence of retarding agents: an in situ high energy X-ray diffraction study. Ind. Chem. Eng. Res. 44 (2005) 5579-5584
23. Meller N., Hall C., Jupe A.C., Colston S.L., Jacques S., Barnes P., and Phipps J. Time resolved studies of the hydration of brownmillerite with and without gypsum: a synchrotron diffraction study at ambient and elevated temperature. J. Mater. Chem. 14 3 (2004) 428-435
24. Shaw S., Henderson C.M.B., and Clark S.M. Hydrothermal synthesis of cement phases: an in situ synchrotron energy dispersive diffraction study of reaction kinetics and mechanisms. High Press. Res. 20 (2001) 311-3204
25. Jupe A.C., Turrillas X., Barnes P., Colston S.L., Hall C., Häusermann D., and Hanfland M. Fast in situ X-ray diffraction studies of chemical reaction: a synchrotron view of the hydration of tricalcium aluminate. Phys. Rev. 53 (1996) 14697-14700
26. Meredith P., Donald A.M., Meller N., and Hall C. Tricalcium aluminate hydration: microstructural observation by in situ electron microscopy. J. Mater. Sci. 39 3 (2004) 997-1005
27. 2O systems. Adv. Cem. Res. 11 4 (1999) 179-187
28. 2O system treated hydrothermally. Thermochim. Acta 334 (1999) 115-122
29. Lupo F., Cockroft J.K., Barnes P., Stukas P., Vickers M., Norman C., and Bradshaw H. Hydrothermal crystallisation of doped zirconia: an in-situ X-ray diffraction study. Phys. Chem. Chem. Phys. 6 8 (2004) 1837-1841
30. F. Lupo, Studies on crystallisation of zirconia under hydrothermal conditions, PhD Thesis, University of London, 2002.
31. Barnes P., Jupe A.C., Colston S.L., Jacques S., Grant A., Rathbone T., Miller F.M., Clark S.M., and Cernik R.J. A new three-angle energy-dispersive diffractometer. Nucl. Instrum. Methods Phys. Res., B Beam Interact. Mater. Atoms 134 (1998) 310-313
32. Colston S.L., Barnes P., Jupe A.C., Jacques S., Hall C., Livesey P., Dransfield J., and Meller N. An in situ synchrotron energy-dispersive diffraction study of the hydration of oilwell cement systems under high temperature/autoclave conditions up to 130 °C. Cem. Concr. Res. 35 12 (2005) 2223-2232
33. 2 with quartz in connection with coal demineralisation. Ind. Eng. Chem. Res. 36 (1997) 1464-1469
34. Hu X., Yanagisawa K., Onda A., and Kajiyoshi K. Stability and phase relations of dicalcium silicate hydrates under hydrothermal conditions. J. Ceram. Soc. Jpn. 114 2 (2006) 174-179
35. Bensted J. Thickening behaviour of oilwell cement slurries with silica flour and silica sand additions. Chem. Ind. 18 (1992) 702-704