Separation and identification of the fifteen constituents in forsythiae fructus

Journal of Food and Drug Analysis

Volumn 15, Issue 1, 2007, Pages 33-39

  Huang, Wen Ying ^a   Sheu, Shuenn Jyi ^a  

^a NATIONAL TAIWAN NORMAL UNIVERSITY   (Taiwan)

Author keywords

Constituent separation; Forsythiae fructus; High performance liquid chromatography; LC MS

Indexed keywords

ACETIC ACID; ACETONITRILE; ACTEOSIDE; ARCTIGENIN; ARCTIIN; CORNOSIDE; FORSYTHIA EXTRACT; FORSYTHIASIDE; HERBACEOUS AGENT; MATAIRESINOL; MATAIRESINOSIDE; METHANOL; PHILLYRIN; PHOSPHATE; PINORESINOL; PINORESINOL BETA DEXTRO GLUCOSIDE; QUERCITRIN; RENGYOSIDE B; RENGYOSIDE C; SALIDROSID; SUSPENSASIDE; UNCLASSIFIED DRUG;

ABSORPTION; ARTICLE; CALIBRATION; CHINESE MEDICINE; CONCENTRATION RESPONSE; DRUG DETERMINATION; DRUG STRUCTURE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; OLEACEAE; PLANT SEED; REPRODUCIBILITY; SEPARATION TECHNIQUE; ULTRAVIOLET RADIATION;

OLEACEAE;

EID: 34249061411     PISSN: 10219498     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (23)

1. Ishizuka, O., Kumazawa, N., Ohta, S., Kamogawa, A. and Shinoda, M. 1992. Effects of various methanol extracts of crude drugs on experimental subacute and chronic hepatic injury. Yakugaku Zasshi 112: 174-182.
2. Jiansu New Medical College. 1999. Zhong Yao Da Ci Dian. pp. 1028, 5457-5458. Shanghai Kexue Jishu Pub. Shanghai.
3. Hsu, H. Y., Chen, Y. P., Sheu, S. J., Hsu, C. H., Chen, C. C. and Chang, H. C. 1985. Chinese Materia Medica - A Concise Guide. pp. 144-145. Modern Drug Press. Taipei, Taiwan, R. O. C.
4. Schinella, G. R., Tournier, H. A., Prieto, J. M., Mordujovich de Buschiazzo, P. and Rios, J. L. 2002. Antioxidant activity of anti-inflammatory plant extracts. Life Sci. 70: 1023-1033.
5. Kinoshita, K., Kawai, T., Imaizumi, T., Akita, Y., Koyama, K. and Takahashi, K. 2004. Soil nutrient factors related to salidroside production of Rhodiola sachalinensis distributed in Chang Bai Mountain. Environ. Exp. Bot. 52: 267-276.
6. Cuellar, M. J., Giner, R. M., Recio, M. C., Just, M. J., Manez, S., Cerda, S. and Rios, J. L. 1998. Screening of antiinflammatory medicinal plants used in traditional medicine against skin diseases. Phytother. Res. 12: 18-23.
7. Ozaki, Y., Rui, J., Tang, Y. and Satake, M. 1997. Antiinflammatory effect of Forsythia suspensa Vahl and its active fraction. Biol. Pharm. Bull. 20: 861-864.
8. Takasaki, M., Konoshima, T., Katsuko, K., Tokuda, H. and Nishno, H. 2000. Anti-tumor-promoting activity of lignans from the aerial part of Saussurea medusa. Cancer Lett. 158: 53-59.
9. Nishibe, S., Okabe, K., Tsukamoto, H., Sakushima, A., Hisada, S., Baba, H. and Akisada, T. 1992. Studies on the Chinese crude drug "Forsythiae Fructus". VI. The structure and antibacterial activity of suspensaside isolated from Forsythia suspensa. Chem. Pharm. Bull. 30: 4548-4553.
10. Kim, N. Y., Kang, T. H., Song, E. K., Pae, H. O., Chung, H. T. and Kim, Y. C. 2000. Inhibitory effects of butanol fraction of the aqueous extract of Forsythia koreana on the nitric oxide production by murine macrophage-like RAW 264.7 cells. J. Ethnopharmacol. 73: 323-327.
11. Chen, Y., Zhu, B. H. and Fang, J. H. 2002. Determination of forsythin in Shuanghuanglian Oral Liquid by RP-HPLC. Chin. Trad. Pat. Med. 24: 761-763.
12. Li, H. B. and Chen, F. 2001. Preparative isolation and purification of salidroside from the Chinese medicinal plant Rhodiola sachalinensis by high-speed counter-current chromatography. J. Chromatogr. A 932: 91-95.
13. Cui, Y. Y., Feng, G. Z. and Wang, M. Z. 1992. HPLC analysis of the active ingredients of Forsythia suspense. Yao Xue Xue Bao. 27: 603-608.
14. Shoeb, M., Celik, S., Jaspars, M., Kumarasamy, Y., MacManus, S. M., Nahar, L., Thoo-Lind, P. K. and Sarkere, S. D. 2005. Isolation, structure elucidation and bioactivity of schischkiniin, a unique indole alkaloid from the seeds of Centaurea schischkinii. Tetrahedron 61: 9001-9006.
15. Yuan, X., Koh, H. L. and Chui, W. K. 2005. A high-performance liquid chromatography method for the simultaneous determination of arctiin, chlorogenic acid and glycyrrhizin in a Chinese proprietary medicine. J. Pharm. Biomed. Anal. 39: 697-704
16. Han, X., Zhang, T., Wei, Y., Cao X. and Ito, Y. 2002. Separation of salidroside from Rhodiola crenulata by high-speed counter-current chromatography. J. Chromatogr. A 971: 237-241.
17. Soriente, A., Rocca, A. D. and Sodano, G. 1997. Chemo-enzymatic synthesis of rengyoside -A, -B, isorengyoside and synthesis of their aglycones. Tetrahedron 53: 4693-4702.
18. Milder, I. J., Arts, I. C. W., Venema, D. P., Lasaroms, J. J. P., Kristina, W. and Hollman, P. C. H. 2004. Optimization of a liquid chromatography-tandem mass spectrometry method for quantification of the plant lignans secoisolariciresinol, matairesinol, lariciresinol, and pinoresinol in foods. J. Agric. Food Chem. 52: 643-4651.
19. Smelcerovic, A., Spiteller, M. and Zuehlke, S. 2006. Comparison of methods for the exhaustive extraction of hypericins, flavonoids, and hyperforin from Hypericum perforatum L. J. Agric. Food Chem. 54: 2750-2753.
20. Nishibe, S. 2002. The plant origins of herbal medicines and their quality evaluation. Yakugaku Zasshi 122: 363-379.
21. Jensen, S. R., Franzyk, H. and Wallander, E. 2002. Chemotaxonomy of the Oleaceae: iridoids as taxonomic markers. Phytochemistry 60: 213-231.
22. Li, L., Tsao, R., Liu, Z., Liu, S., Yang, R., Young, J. C., Zhu, H., Deng, Z., Xie, M. and Fu, Z. 2005. Isolation and purification of acteoside and isoacteoside from Plantago psyllium L. by high-speed counter-current chromatography. J. Chromatogr. A 1063: 161-169.
23. Schmidt, T. J., Stausberg, S., Raison, J. V., Berner, M. and Willuhn, G. 2006. Lignans from Arnica species. Nat. Prod. Res. 20: 443-453.