Simultaneous qualification and quantification of eight triterpenoids in Radix Achyranthis Bidentatae by high-performance liquid chromatography with evaporative light scattering detection and mass spectrometric detection

Journal of Separation Science

Volumn 30, Issue 6, 2007, Pages 843-850

  Li, Juan ^a   Li, Ping ^a   Li, Hui Jun ^a   Song, Yue ^a   Bi, Zhi Ming ^a   Li, Yan Jing ^a  

^a CHINA PHARMACEUTICAL UNIVERSITY   (China)

Author keywords

Genuine crude drug; HPLC ELSD; HPLC MS; Radix Achyranthis Bidentatae; Triterpenoids

Indexed keywords

LIGHT SCATTERING; LINEAR REGRESSION; MASS SPECTROMETRY; MEDICINE; NITROGEN;

EVAPORATIVE LIGHT SCATTERING DETECTION; GENUINE CRUDE DRUG;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

ACETONITRILE; ACHYRANTHES BIDENTATA EXTRACT; CHIKUSETSU SAPONIN; FORMIC ACID; NITROGEN; TRITERPENOID;

ACHYRANTHES; ACHYRANTHES BIDENTATA; AQUEOUS SOLUTION; ARTICLE; CHEMICAL COMPOSITION; CONTROLLED STUDY; DRUG STRUCTURE; ELUTION; EVAPORATION; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIGHT SCATTERING; LINEAR REGRESSION ANALYSIS; MASS SPECTROMETRY; PRIORITY JOURNAL; QUALITATIVE ANALYSIS; QUALITY CONTROL; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; SENSITIVITY ANALYSIS; TEMPERATURE; VALIDATION STUDY;

ACHYRANTHES; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DRUGS, CHINESE HERBAL; GINSENOSIDES; MOLECULAR STRUCTURE; OLEANOLIC ACID; PLANT ROOTS; REPRODUCIBILITY OF RESULTS; SAPONINS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TRITERPENES;

EID: 34248349495     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200600341     Document Type: Article

References (17)

1. Pharmacopoeia of the People's Republic of China, Chemical Industry Press, Peking 2005, p. 49.
2. Meng, D. L., Li, X., Chin. J. Med. Chem. 2001, 11, 120-124.
3. Xu, X. X., Kong, S.J., J. Anhui TCM College 2005, 24, 63-64.
4. Li, X. D., Hu, S. L., China J. Chin. Mater. Med. 1995, 20, 459-460.
5. Zhang, Q. W., Chin. Pham. J. 1995, 30, 592-594.
6. Jiang, C. M., Xu, J. D., Wang, H. Q., Chin. J. Mod. Appl. Pharm. 1998, 15, 22-24.
7. Chen, H. L., Wang, J. K., Zhang, L. L., Chin. J. Chin. Mater. Med. 1997, 22, 281-283.
8. Li, H. J., Li, P., Ye, W. C., J. Chromatogr. A 2003, 1008, 167-172.
9. Li, P., Zheng, L. J., Li, S. L., Acta Pharm. Sin. 2004, 39, 56-59.
10. Chai, X. Y., Li, S. L., Li, P., J. Chromatogr. A 2005, 1070, 43-48.
11. Liao, L. P., Li, S. L., Li, P., J. Sep. Sci. 2005, 28, 2061-2066.
12. Romussi, G., Bignardi, G., Arch. Pharm. 1987, 320, 153-158.
13. Nie, R. L., Morita, T., Kasai, R., Planta Med. 1984, 50, 322-327.
14. Wang, X. J., Zhu, L. Z., J. Fourth Mil. Med. Univ. 1996, 17, 427-430.
15. Meng, D. L., Li, X., Xiong, Y. H., J. Shenyang Pharm. Univ. 2002, 19, 27-30.
16. Hu, M., Ogawa, K., Sashida, Y., Xiao, P. G., Phytochemistry 1995, 39, 179-184.
17. Alltech ELSD 2000 Operating Manual, Alltech 2001, p. 16 (in Chinese).