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The reaction was performed with (diethylamino)sulfur trifluoride (DAST) in dichloromethane at -80 °C
-
DMB fluoride was prepared by substitution of the hydroxyl group of DMB (ref 3a) by fluorine
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DMB fluoride was prepared by substitution of the hydroxyl group of DMB (ref 3a) by fluorine. The reaction was performed with (diethylamino)sulfur trifluoride (DAST) in dichloromethane at -80 °C. The product was purified by column chromatography (silica gel, dichloromethane).
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The product was purified by column chromatography (silica gel, dichloromethane)
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19
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34247572884
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The amount of conversion was determined by GC/MS analysis, actinometry was done with ferrioxalate. The standard error defines reproducibility
-
The amount of conversion was determined by GC/MS analysis, actinometry was done with ferrioxalate. The standard error defines reproducibility.
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20
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13444312005
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Gaplovsky, M.; Il'ichev, Y. V.; Kamdzhilov, Y.; Kombarova, S.; Mac, M.; Schwörer, M. A.; Wirz, J. Photochem. Photobiol. Sci. 2005, 4, 33-42.
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21
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34247647452
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The rate constant is not accurately defined, because the reaction end point is not reached at the end of the delay line 1.85 ns
-
The rate constant is not accurately defined, because the reaction end point is not reached at the end of the delay line (1.85 ns).
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23
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0033601068
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(b) Newcomb, M.; Horner, J. H.; Whitted, P. O.; Crich, D.; Huang, X.; Yao, Q.; Zipse, H. J. Am. Chem. Soc. 1999, 121, 10685-10694.
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0033552267
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1,3-Diphenyl-1,3-cyclopentanediyl radicals absorb at 320 nm: Kita, F.; Adam, W.; Jordan, P.; Nau, W. M.; Wirz, J. J. Am. Chem. Soc. 1999, 121, 9265-9275.
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1,3-Diphenyl-1,3-cyclopentanediyl radicals absorb at 320 nm: Kita, F.; Adam, W.; Jordan, P.; Nau, W. M.; Wirz, J. J. Am. Chem. Soc. 1999, 121, 9265-9275.
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27
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34247569373
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Rock and Chan gave a lower limit of 5 ps for the lifetime of intermediate D assuming diffusion-controlled reaction with water.
-
Rock and Chan gave a lower limit of 5 ps for the lifetime of intermediate D assuming diffusion-controlled reaction with water.
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