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3 in liquid state show a triplet; in spectrum a of Figure 2 only a singlet is shown because we used a solid state probe for liquid analysis, and this has produced a loss of resolution.
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A qualitative evaluation of the length of the polyethylene oxide chains formed upon epoxy opening can be obtained looking at 13C signal in the 70-74 ppm range. The formation of short oligomeric ethylene oxide chains of different length is generally revealed by the presence of overlapped sharp signals, and a broad signal is instead an indication of longer chains
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13C signal in the 70-74 ppm range. The formation of short oligomeric ethylene oxide chains of different length is generally revealed by the presence of overlapped sharp signals, and a broad signal is instead an indication of longer chains.
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