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51
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34247534994
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-1 (Cu Kα, λ = 1.54178 Å), T = 293 K. R1 = 0.0431 and wR2 = 0.1335 for 3034 unique reflections > 2σ(I).
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-1 (Cu Kα, λ = 1.54178 Å), T = 293 K. R1 = 0.0431 and wR2 = 0.1335 for 3034 unique reflections > 2σ(I).
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-
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52
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34247474837
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-1 (Cu Kα, λ = 1.54178 Å), T = 293 K. R1 = 0.0376 and wR2 = 0.1195 for 4065 unique reflections > 2σ(I).
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-1 (Cu Kα, λ = 1.54178 Å), T = 293 K. R1 = 0.0376 and wR2 = 0.1195 for 4065 unique reflections > 2σ(I).
-
-
-
-
54
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34247465138
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-1(Cu Kα, λ = 1.54178 Å), T= 293 K. R1 = 0.0718 and wR2 = 0.2041 for 11934 unique reflections > 2σ(I).
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-1(Cu Kα, λ = 1.54178 Å), T= 293 K. R1 = 0.0718 and wR2 = 0.2041 for 11934 unique reflections > 2σ(I).
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55
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34247546645
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Crystal data for 6: C23H25N 2O2Br, M, 441.37, triclinic, space group P1, a, 6.8268(8) Å, b, 12.5858(14) Å, c, 14.2335(16) Å, α, 79.547-(7)°, β, 12.5858(14)°, γ, 14.2335(16)°. V, 1158.2(2) Å3, Z, 2, Ocalcd, 1.266 g cm-3, m, 2.564 mm-1 (Cu Kα, λ, 1.54178 Å, T, 293 K. R1, 0.0537 and wR2, 0.1518 for 4068 unique reflections > 2σI
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-1 (Cu Kα, λ = 1.54178 Å), T = 293 K. R1 = 0.0537 and wR2 = 0.1518 for 4068 unique reflections > 2σ(I).
-
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56
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34247476785
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-1, respectively.
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-1, respectively.
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