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Volumn 36, Issue 2, 2007, Pages 276-277

Azaspirovesamicols - Regioselective synthesis and crystal structure analysis of a novel class of vesamicol analogues as potential ligands for the vesicular acetylcholine transporter

(4) Wenzel, Barbara a Bats, Jan W b Scheunemann, Matthias a Steinbach, Jörg a

a Institut fur Interdisziplinare Isotopenforschung (Germany)

b GOETHE UNIVERSITY (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 34247262121 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2007.276 Document Type: Article

Times cited : (3)

References (13)

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- The structures were determined by direct methods and refined by least-squares against all measured F2 values.10 5a: C28H36N2O2, M r, 432.59, triclinic, PĪ1 (no. 2, a, 6.1634(9, b, 9.970(3, c, 19.717(3) Å, α, 86.432(12, β= 84.113(11, γ, 76.328(19)°, V, 1170.2(4) Å, 3 Z= 2, T =149K, Dcalcd, 1.228gern-3, μ, 0.077 mm-1, 15658 refections measured, 6911 unique reflections, Rint, 0.024, 294 refined parameters, R1(F, I > 2σ(I, 0.043, GOF, 1.05; 5b: C28H37N2O 2+ Cl, Mr, Mr= 469.05, orthorhombic, Pca21 (no. 29, a, 14.439(4, b, 8.8908(18, c, 39.195(8)A, V, 50
- 1(F) [I > 2σ(I)] = 0.082, GOF =1.05. Crystallographic data reported in this manuscript have been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 624382 (5a) and CCDC 624383 (5b). Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk./conts/ retrieving.html.

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13
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- Supporting information is available electronically on the CSJ-Joumal Web site http://www.csj.jp/journals/chem-lett/index.html.
- Supporting information is available electronically on the CSJ-Joumal Web site http://www.csj.jp/journals/chem-lett/index.html.

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