Structure and vibrational dynamics of isotopically labeled lithium borohydride using neutron diffraction and spectroscopy

Journal of Solid State Chemistry

Volumn 180, Issue 4, 2007, Pages 1298-1305

  Hartman, Michael R ^a   Rush, John J ^a   Udovic, Terrence J ^a   Bowman Jr , Robert C ^b   Hwang, Son Jong ^c  

^a NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

^b CALIFORNIA INSTITUTE OF TECHNOLOGY   (United States)

^c California Institute of Technology   (United States)

Author keywords

Hydrogen storage; Lithium borohydride; Neutron scattering; NMR

Indexed keywords

HYDROGEN STORAGE; MICROSTRUCTURE; NEUTRON DIFFRACTION; NUCLEAR MAGNETIC RESONANCE; VIBRATION ANALYSIS;

ATOMIC DISPLACEMENT; LITHIUM BOROHYDRIDE; REORIENTATIONAL MOTIONS;

LITHIUM COMPOUNDS;

EID: 34247248195     PISSN: 00224596     EISSN: 1095726X     Source Type: Journal    
DOI: 10.1016/j.jssc.2007.01.031     Document Type: Article

References (22)

1. Züttel A., Wenger P., Rentsch S., Sudan P., Mauron Ph., and Emmenegger Ch. J. Power Sources 118 (2003) 1-7
2. Nakamori Y., and Orimo S. J. Alloy Compd. 370 (2004) 271-275
3. Vajo J., Skeith S., and Mertens F. J. Phys. Chem. B 109 (2005) 3719-3722
4. Schlesinger H.I., and Brown H.C. J. Am. Chem. Soc. 62 (1940) 3429-3435
5. Harris P.M., and Meibohm E.P. J. Am. Chem. Soc. 69 (1947) 1231-1232
6. Soulié J.-Ph., Renaudin G., Černý R., and Yvon K. J. Alloy Compd. 346 (2002) 200-205
7. Hagemann H., Gomes S., Renaudin G., and Yvon K. J. Alloy Compd. 363 (2004) 126-129
8. Tsang T., and Farrar T.C. J. Chem. Phys. 50 (1969) 3498-3502
9. Schlesinger H.I., Brown H.C., Mayfield D.L., and Gilbreath J.R. J. Am. Chem. Soc. 75 (1953) 213-215
10. Schlesinger H.I., Brown H.C., and Finholt A.E. J. Am. Chem. Soc. 75 (1953) 205-209
11. Brown H.C., Choi Y.M., and Narasimhan S. Inorg. Chem. 21 (1982) 3657-3661
12. Brown H.C. Organic Syntheses via Boranes (1975), Wiley, New York
13. Certain commercial firms and trade names are identified in this report in order to specify aspects of the experimental procedure adequately. Such identification is not intended to imply recommendation or endorsement by the National Institute of Standards and Technology, nor is it intended to imply that the materials for equipment identified are necessarily the best available for the purpose
14. X-ray diffraction studies were conducted on a Bruker Advanced X-ray Solutions D8 Advance diffractometer using CuKα radiation. Air sensitive materials were sealed in quartz capillaries
15. Infrared spectroscopy studies were performed on a Thermo Nicolet Nexus 670 FT-IR Spectrometer.
16. A.C. Larson, R.B. Von Dreele, General structure analysis system (GSAS), Los Alamos National Laboratory Report LAUR 86-748, 2000.
17. Toby B.H. J. Appl. Crystallogr. 34 (2001) 210-213
18. Udovic T.J., Neumann D.A., Leão J., and Brown C.M. Nucl. Instrum. Methods Phys. Res. A 517 (2004) 189-201
19. Busing W.R., and Levy H.A. Acta Crystallogr. 17 (1964) 142-146
20. Renaudin G., Gomes S., Hagemann H., Keller L., and Yvon K. J. Alloy Compd. 375 (2004) 98-106
21. Tomkinson J., and Waddington T.C. J. Chem. Soc. Faraday Trans. 72 (1976) 528-538
22. Gomes S., Hagemann H., and Yvon K. J. Alloy Compd. 346 (2002) 206-210