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Volumn 3, Issue 1, 2006, Pages 25-28

Facile and selective preparation of esters from carboxylic acids catalyzed by aluminumdodecatangstophosphate (AlPW12O40) as a versatile, recyclable and a highly water tolerant green Lewis acid catalyst

(3) Firouzabadi, Habib a Iranpoor, Nasser a Jafari, Abbas Ali a

a SHIRAZ UNIVERSITY (Iran)

Author keywords

Alcohols; AlPW12O40; Aluminumdodecatungstophosphate; Carboxylic acids; Esterfication

Indexed keywords

EID: 34247237881 PISSN: 15701786 EISSN: None Source Type: Journal
DOI: 10.2174/157017806774964495 Document Type: Article

Times cited : (11)

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36
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- Typical esterification procedure: In a typical experiment, esterification of phenylacetic acid (5 mmol, 0.68g) and 1-butanol (10 mmol, ∼1 ml) was carried out in a 100 ml round bottom flask with 10 M0l% of AlPW12 O40 powder. The reaction mixture was stirred at 75-80°C for 0.3h. Ethyl acetate (100 ml) was added to the reaction mixture, filtered and washed with ethyl acetate to recover the catalyst. The solvent and the unreacted butanol were evaporated off. The pure ester was obtained in 96% yield (1.84g) and identified by its IR, 1H NMR, and 13C NMR spectral data. Selected analytical data for n-butyl phenylacetate (Table 1, Entry3, 1H NMR (250 MHz, CDCl3, δ(ppm, 7.25 (s, 5H, 4.06 (t, 2H, J=6.65 Hz, 3.57 (s, 2H, 1.60-1.50 (m, 2H, 1.36-1.27 (m, 2H, 0.91-0.85 (t, 3H, J=7.5 Hz, 13C NMR (CDCl3, 63MHz) δ ppm, 172, 133.2, 129.6, 128.9, 127.4, 65.1, 41.8, 3
- +.

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