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Volumn 36, Issue 1, 2007, Pages 150-151

Zinc(II) and copper(I)-ferrocenedicarboxylate polyhedron and polygon

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EID: 34247237812 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2007.150 Document Type: Article

Times cited : (9)

References (13)

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8
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- Kondo, M.¹ Shinagawa, R.² Miyazawa, M.³ Kabir, M.K.⁴ Irie, Y.⁵ Horiba, T.⁶ Naito, T.⁷ Maeda, K.⁸ Utsuno, S.⁹ Uchida, F.¹⁰

9
- 34247279223
- Typical procedure: [Zn6O2(FDCA) 5(H2O)(DMF)]·4DMF (1, DMF solution (10mL) containing 1,1′-ferrocenedicarboxylic acid (H2FDCA, 55 mg, 0.20 mmol) and Zn(NO3)2· 6H2O (60 mg, 0.20 mmol) was diffused by triethylamine (0.2 mL) in DMF (2 mL) for 2 weeks. The black block crystals were isolated to give 21 mg (25, Anal. Calcd for C 75H77O28-N5Fe5Zn 6: C, 41.54; H, 3.59; N, 3.23, Found: C, 41.88; H, 3.63; N, 3.48, FT-IR (KBr, cm-1, 1637(m, 1571(s, 1490(vs, 1403(s, 1368m
- -1): 1637(m), 1571(s), 1490(vs), 1403(s), 1368(m).

10
- 34247200495
- Zn8O4(FDCA)6(H2O) 3]· 4DMA·2H2O (2, Solution (1.8mL) of an equal amount of DMA and ethanol containing H2FDCA (18 mg, 0.07 mmol) and Zn(NO3)2·6H2O (21 mg, 0.07mmol) was heated at 83°C for 10h and then cooled to room temperature. The resulting mixture was again heated to 93°C for 12h. The dark red cubic crystals were obtained (9mg, 32, Anal. Calcd for C88H94O 37N3Fe6Zn8: C, 39.76; H, 3.57; N, 2.11, Found: C, 39.84; H, 3.48; N, 2.15, FT-IR (KBr, cm-1, 1663(s, 1576(s, 1490(vs, 1388(vs, 1357m
- -1): 1663(s), 1576(s), 1490(vs), 1388(vs), 1357(m).

11
- 34247184708
- Cu4(FDCA)2, 3, DMA solution (1.4mL) of H 2FDCA (5.5mg, 0.02 mmol) and Cu(NO3)2· 3H2O (4.8 mg, 0.02mol) was placed in a Pyrex tube and heated at 80°C for 12h. The pale yellow plate crystals were obtained (9mg, 56, Anal. Calcd for C24H16O8Cu4Fe 2: C, 36.11; H, 2.02, Found C, 36.06; H, 2.03, FT-IR (KBr, cm -1, 1658(w, 1576(sh, 1545 (vs, 1495(vs, 1403(vs, 1367s
- -1): 1658(w), 1576(sh), 1545 (vs), 1495(vs), 1403(vs), 1367(s).

12
- 34247230209
- Crystal Data. All measurements were made on a SMART CCD area detector with graphite-monochromated MoKα radiation: [Zn6O 2(FDCA)5(H2O)(DMF)]·4DMF (1, monoclinic, space group P21/n, a=15.0363(13, b, 22.620(2, c, 23.0084(17)Å, α, 90°, β= 98.511(3)°, γ, 90°, V, 7739.6(11)Å3, Z, 4, Dcalcd, 0.766 Mg/m3, μ, 0.907 mm-1, 1.43° ≤ θ ≤ 27.44°, 25 ≤ h ≤ 25, 24 ≤ k ≤ 26, 25 ≤ l ≤ 24. Total of 53100 reflections, unique 3029. R1, 0.0962 with I > 2σ(I, wR2, 0.2729, GOF, 0.862. CCDC-622019, Zn8O4(FDCA) 6(H2O)3·4DMA·2H2O (2, cubic, space group Pa(3̄, a, 26.1553(5) Å, α, 90°, V, 17892.8(6) Å3, Z, 8, Dcalcd, 1.813 Mg/m 3, μ, 2.81
- 1 = 0.0624 with I > 2σ(I), wR2 = 0.1067, GOF = 0.987. CCDC-622018.

13
- 34247193050
- Better descriptions of polyhedra are shown in Figures S1 and S2.
- Better descriptions of polyhedra are shown in Figures S1 and S2.

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