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Volumn 36, Issue 2, 2007, Pages 234-235

Four kinds of 21 helical assemblies with the molecular tilt as well as three-directional and facial chirality

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EID: 34247212304 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2007.234 Document Type: Article

Times cited : (13)

References (21)

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19
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- Crystallographic data for brucinium 3,5-di-tert-butyl-4- hydroxybenzoate (1·2) acetone solvate from acetone solution; 2C 23H27-N2O4·2C 15H21O3·C3H6O, MW 1347.69, monoclinic, P21, 4, a, 14.8933(6, b, 12.9949(5, c, 18.6164(8) Å, β, 100.496(2)°, V, 3542.7(2) Å3, Z, 2, Dcalcd, 1.263 g cm-3, 2θMAX, 136.4°, 24773/11406 measure/independent reflections, R= 16.53, Rw, 38.51
- MAX = 136.4°, 24773/11406 measure/independent reflections, R= 16.53, Rw = 38.51.

20
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- MAX = 136.5°, 10441/4111 measure/independent reflections, R = 6.49, Rw = 21.51. Crystallographic data reported in this manuscript have been deposited with Cambridge Crystallographic Data Centre as supplementary publication Nos. CCDC-629249 and -629250. Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/ retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 1EZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk).
- MAX = 136.5°, 10441/4111 measure/independent reflections, R = 6.49, Rw = 21.51. Crystallographic data reported in this manuscript have been deposited with Cambridge Crystallographic Data Centre as supplementary publication Nos. CCDC-629249 and -629250. Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/ retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 1EZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk).

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