Validation of high-performance liquid chromatography assay for quantification of formoterol in urine samples after inhalation using UV detection technique

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 850, Issue 1-2, 2007, Pages 31-37

  Nadarassan, D K ^a   Chrystyn, H ^a   Clark, B J ^a   Assi, K H ^a  

^a UNIVERSITY OF BRADFORD   (United Kingdom)

Author keywords

Assay; Formoterol; HPLC; Validation

Indexed keywords

ACETONITRILE; ALCOHOLS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PH EFFECTS; PHOSPHORIC ACID; ULTRAVIOLET DETECTORS;

FORMOTEROL; SOLID PHASE EXTRACTION (SPE); URINE MATRIX; VALIDATION;

BIOASSAY;

ACETONITRILE; FORMOTEROL; POTASSIUM DIHYDROGEN PHOSPHATE;

ARTICLE; CONTROLLED STUDY; DRUG ISOLATION; DRUG URINE LEVEL; FEMALE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; MALE; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; ULTRAVIOLET RADIATION; URINALYSIS;

ADMINISTRATION, INHALATION; ADRENERGIC BETA-ANTAGONISTS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; ETHANOLAMINES; HUMANS; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SPECTROPHOTOMETRY, ULTRAVIOLET;

EID: 34247191285     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2006.10.059     Document Type: Article

References (31)

1. The Merck Index, 12th ed., 1996, p. 4272.
2. Cherkaoui S., Faupel M., and Francotte E. J. Chromatogr. A 715 (1999) 132
3. Benhamou D., Cuvelier A., Muir J.F., Leclerc V., Le Gros V., Kottakis J., and Bourdei I. Respir. Med. 95 (2001) 817
4. Faulds D., Hollingshead L.M., and Goa K.L. Drugs 42 (1991) 115
5. Fozard J.R., and Buescher H. Pulm. Pharmacol. Ther. 14 4 (2001) 289
6. Bartow R.A., and Brogden R.N. Drug 55 (1998) 303 Abstract-EMASE/Abstract-MEDLINE
7. SIGN, Pharmacological Management of Asthma, Evidence Table 4.11b: Add-on Drugs for Inhaled Steroids: Long Acting or Oral B2 Agonists, 2002, website http://www.sign.ac.uk/guidelines/published/support/guideline63/index.html.
8. Pauwels R.A., Löfdahl C.-G., Postma D.S., Tattersfield A.E., O'Byrne P., Barnes P.J., and Ullman A. Additive effects of inhaled formoterol and budesonide in reducing asthma exacerbations: a one-year, controlled study. New Engl. J. Med. 337 (1997) 1405-1411
9. Lecaillon J.B., Kaiser G., Palmisano M., Morgan J., and Cioppa G.D. Eur. J. Clin. Pharmacol. 55 (1999) 131
10. Song J.Z., Chen J., Tian S.J., and Sun Z.P. J. Pharm. Biomed. Anal. 21 (1999) 569
11. Campestrini J., Lecaillon J.B., and Godbillion J. J. Chromatogr. B 704 (1997) 221
12. Graham S.J., Beaulieu N., and Lovering E.G. J. Liq. Chromatogr. 16 (1993) 1497
13. Marzo A., Monti N.C., Tettamanti R.A., Crivelli F., Dal Bo L., Mazzucchelli P., Meoli A., Pezzuto D., and Corsico A. Arzneimittelforschung 50 (2000) 559
14. Kamimura H., Sasaki H., Higichi S., and Shiobara Y. J. Chromatogr. Biomed. Appl. 229 (1982) 337
15. Damasceno L., Ventura R., Cardoso J., and Segura J. J. Chromatogr. B 780 (2002) 61
16. Hennion M.C. J. Chromatogr. A 856 (1999) 3
17. Guidance to Industry: Bioanalytical Method Validation US Department of Health and Human Services FDA, CDER, CVM, May 2001, website http://www.fda.gov/cder/guidance/index.htm.
18. Validation of Analytical Procedures: Methodology Q2B, ICH Steering Committee, 6 November 1996, website http://www.ich.org/.
19. Validation of Analytical Procedures Q2A, ICH Steering Committee, 27 October 1994, website http://www.ich.org/.
20. Shah V.P., Midha K.K., Findlay J.W., Hill H.M., Hulse J.D., McGilveray I.J., McKay G., Miller K.J., Patnaik R.N., Powell M.L., Tonelli A., Viswanathan C.T., and Yacobi A. Pharm. Res. 17 (2000) 1551
21. S. Levin, Analytical Department Medtechnica Handouts: Sample Preparation Using Solid Phase Extraction, website http://forumsci.co.il/HPLC.
22. ® HLB Chemistry, website http://www.waters.com.
23. Bidlingmeyer B.A. J. Chromatogr. Sci. 18 (1980) 525
24. Waters Associates, Bulletin No. N80, 1981.
25. Walshe M., Kelly M.T., Smyth M.R., and Ritchie H. J. Chromatogr. A 708 (1995) 31
26. Assi K.H., Tarsin W., and Chrystyn H. J. Pharm. Biomed. Anal. 41 (2006) 325
27. Rosenborg J., et al. Eur. Respir. J. 14 Suppl. 30 (1999) 62
28. Firkusny L., et al. Klin. Wochenschr. 68 Suppl. 19 (1990) 42
29. Chrystyn H. Br. J. Clin. Pharmacol. 51 (2001) 289
30. Akapo S.O. J. Pharm. Biomed. Anal. 33 (2003) 935
31. Ong H., et al. J. Chromatogr. 497 (1989) 213