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Synlett

Volumn , Issue 6, 2007, Pages 897-900

Palladium-catalyzed naphthylation of acenaphthylene

(4) Dyker, Gerald a Merz, Klaus a Oppel, Iris M a Muth, Enrico a

a RUHR UNIVERSITY BOCHUM (Germany)

Author keywords

Annulated cyclopentadienes; Heck reaction; Hydrocarbons; Palladium; Polycyclic aromatic

Indexed keywords

ACENAPTHYLENE; PALLADIUM; UNCLASSIFIED DRUG;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CATALYSIS; CHEMICAL BOND; CHEMICAL MODIFICATION; CHEMICAL STRESS; CYCLIZATION; DEHYDROCYCLIZATION; HECK REACTION; NAPHTHYLATION; PROTON NUCLEAR MAGNETIC RESONANCE; SYNTHESIS;

EID: 34247109525 PISSN: 09365214 EISSN: None Source Type: Journal
DOI: 10.1055/s-2007-970785 Document Type: Article

Times cited : (13)

References (15)

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- X-ray data for 5 were collected on a Bruker AXS-SMART 1000 (Mo Kα radiation, The structure was solved by direct methods and refined by full matrix least squares using SHELXTL-97 All non-hydrogen atoms were refined using anisotropic thermal parameters. Crystal Data for 5 T, 213(2) K, C32H20, M, 404.48, monoclinic space group P21/n, a, 12.190(5) Å, b, 10.104(4) Å, c, 17.237(7) Å, β, 102.484(9)°, V, 2072.9(15) Å3, Z, 4, DC, 1.296 g/ cm3, μ, 0.073 mm-1, 2.35° < Θ < 25.15°, reflections collected/unique 10788/3646 [Rint, 0.0489, data/restraints/ parameters 3646/0/289, GOF 1.021, final R[I > 2σ(I, R1, 0.0416, wR2 all data, 0.1082, residual density 0.134 and -0.190 e A-3. Crystal Data for
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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.