Detailed elemental compositions of emulsion interfacial material versus parent oil for nine geographically distinct light, medium, and heavy crude oils, detected by negative- and positive-ion electrospray ionization fourier transform ion cyclotron resonance mass spectrometry

Energy and Fuels

Volumn 21, Issue 2, 2007, Pages 973-981

  Stanford, Lateefah A ^a,b   Rodgers, Ryan R ^a,b   Marshall, Alan G ^a,b   Czarnecki, Jan ^c   Wu, Xin A ^c   Taylor, Shawn ^d  

^a FLORIDA STATE UNIVERSITY   (United States)

^b FLORIDA STATE UNIVERSITY   (United States)

^c SYNCRUDE CANADA LTD   (Canada)

^d SCHLUMBERGER   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

ADSORPTION; CHEMICAL ANALYSIS; CYCLOTRON RESONANCE; DENSITY (SPECIFIC GRAVITY); ELECTROSPRAY IONIZATION; EMULSIONS; MASS SPECTROMETRY; STABILIZERS (AGENTS);

EMULSION STABILIZERS; INTERFACE ADSORPTION;

CRUDE PETROLEUM;

EID: 34247099895     PISSN: 08870624     EISSN: None     Source Type: Journal    
DOI: 10.1021/ef060292a     Document Type: Article

References (28)

1. McLean, J. D.; Kilpatrick, P. K. Effects of asphaltene aggregation in model heptane-toluene mixtures on stability of water-in-oil emulsions. J. Colloid Interface Sci. 1997, 196 (1), 23-34.
2. McLean, J. D.; Kilpatrick, P. K. Effects of asphaltene solvency on stability of water-in-crude-oil emulsions. J. Colloid Interface Sci. 1997, 189 (2), 242-253.
3. Acevedo, S.; Escobar, G.; Ranaudo, M. A.; Khazen, J.; Borges, B.; Pereira, J. C.; Mendez, B. Isolation and characterization of low and high molecular weight acidic compounds from Cerro Negro extraheavy crude oil. Role of these acids in the interfacial properties of the crude oil emulsions. Energy Fuels 1999, 13 (2), 333-335.
4. Eley, D. D.; Hey, M. J.; Lee, M. A. Rheological Studies of Asphaltene Films Adsorbed at the Oil-Water Interface. Colloids Surf. 1987, 24 (2-3), 173-182.
5. Sjoblom, J.; Aske, N.; Auflem, I. H.; Brandal, O.; Havre, T. E.; Saether, O.; Westvik, A.; Johnsen, E. E.; Kallevik, H. Our current understanding of water-in-crude oil emulsions. Recent characterization techniques and high pressure performance. Adv. Colloid Interface Sci. 2003, 100, 399-473.
6. Poteau, S.; Argillier, J. F.; Langevin, D.; Pincet, F.; Perez, E. Influence of pH on stability and dynamic properties of asphaltenes and other amphiphilic molecules at the oil-water interface. Energy Fuels 2005, 19 (4), 1337-1341.
7. Hammami, A.; Phelps, C. H.; Monger-McClure, T.; Little, T. M. Asphaltene precipitation from live oils: An experimental investigation of onset conditions and reversibility. Energy Fuels 2000, 14 (1), 14-18.
8. Yarranton, H. W.; Hussein, H.; Masliyah, J. H. Water-in-hydrocarbon emulsions stabilized by asphaltenes at low concentrations. J. Colloid Interface Sci. 2000, 228 (1), 52-63.
9. Zhan, D. L.; Fenn, J. B. Electrospray mass spectrometry of fossil fuels. Int. J. Mass Spectrom. 2000, 194 (2-3), 197-208.
10. Hughey, C. A.; Rodgers, R. P.; Marshall, A. G. Resolution of 11 000 compositionally distinct components in a single electrospray ionization Fourier transform ion cyclotron resonance mass spectrum of crude oil. Anal. Chem. 2002, 74 (16), 4145-4149.
11. Qian, K. N.; Robbins, W. K.; Hughey, C. A.; Cooper, H. J.; Rodgers, R. P.; Marshall, A. G. Resolution and identification of elemental compositions for more than 3000 crude acids in heavy petroleum by negative-ion microelectrospray high-field Fourier transform ion cyclotron resonance mass spectrometry. Energy Fuels 2001, 15 (6), 1505-1511.
12. Wu, X. Investigating the stability mechanism of water-in-diluted bitumen emulsions through isolation and characterization of the stabilizing materials at the interface. Energy Fuels 2003, 17 (1), 179-190.
13. Emmett, M. R.; White, F. M.; Hendrickson, C. L.; Shi, S. D. H.; Marshall, A. G. Application of micro-electrospray liquid chromatography techniques to FT-ICR MS to enable high-sensitivity biological analysis. J. Am Soc. Mass Spectrom. 1998, 9 (4), 333-340.
14. Senko, M. W.; Hendrickson, C. L.; PasaTolic, L.; Marto, J. A.; White, F. M.; Guan, S. H.; Marshall, A. G. Electrospray ionization Fourier transform ion cyclotron resonance at 9.4 T. Rapid Commun. Mass Spectrom. 1996, 10 (14), 1824-1828.
15. Blakney, G. T.; van der Rest, G.; Johnson, J. R.; Freitas, M. A.; Drader, J. J.; Shi, S. D.-H.; Hendrickson, C. L.; Kelleher, N. L.; Marshall, A. G. In Further Improvements to the MIDAS Data Station for FT-ICR Mass Spectrometry, 49th ASMS Conference on Mass Spectrometry and Allied Topics, Chicago, IL, 2001.
16. Senko, M. W.; Hendrickson, C. L.; Emmett, A R.; Shi, S. D. H.; Marshall, A. G. External accumulation of ions for enhanced electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry. J. Am Soc. Mass Spectrom. 1997, 8 (9), 970-976.
17. Hendrickson, C. L.; Quinn, J. P.; Emmett, A R.; Marshall, A. G. In Quadrupole Mays Filtered External Accumulation for Fourier Transform Ion Cyclotron Resonance Mass Spectrometry, 48th ASMS Conference on Mass Spectrometry and Allied Topics, Long Beach, CA, 2000.
18. Ledford, E. B.; Rempel, D. L.; Gross, M. L. Space-charge effects in Fourier-transform mass-spectrometry-mass calibration. 1984, 56 (14), 2744-2748.
19. Shi, S. D. H.; Drader, J. J.; Freitas, M. A.; Hendrickson, C. L.; Marshall, A. G. Comparison and interconversion of the two most common frequency-to-mass calibration functions for Fourier, transform ion cyclotron resonance mass spectrometry. Int. J. Mays Spectrom. 2000, 196, 591-598.
20. Klein, G. C.; Angstrom, A.; Rodgers, R. P.; Marshall, A. G. Use of saturates/aromatics/resins/asphaltenes (SARA) fractionation to determine matrix effects in crude oil analysis by electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry. Energy Fuels 2006, 20 (2), 668-672.
21. Fileti, E. E.; Coutinho, K; Malaspina, T.; Canuto, S. Electronic changes due to thermal disorder of hydrogen bonds in liquids: Pyridine in an aqueous environment. Phys. Rev. E 2003, 67 (6).
22. Nobeli, I.; Price, S. L.; Lommerse, J. P. M.; Taylor, R. Hydrogen bonding properties of oxygen and nitrogen acceptors in aromatic heterocycles. J. Comput. Chem. 1997, 18 (16), 2060-2074.
23. Raevsky, O. A.; Raevskaja, O. E.; Schaper, K. J. Analysis of water solubility data on the basis of HYBOT descriptors. Part 3. Solubility of solid neutral chemicals and drugs. QSAR Comb. Sci. 2004, 23 (5), 327-343.
24. Hampel, M.; Moreno-Garrido, I.; Sobrino, C.; Lubian, L. M.; Blasco, J. Acute toxicity of LAS homologues in marine microalgae: Esterase activity and inhibition growth as endpoints of toxicity. Ecotox. Environ. Saf. 2001, 48 (3), 287-292.
25. Aske, N.; Kallevik, H.; Sjoblom, J. Determination of saturate, aromatic, resin, and asphaltenic (SARA) components in crude oils by means of infrared and near-infrared spectroscopy. Energy Fuels 2001, 15 (5), 1304-1312.
26. Gelot, A.; Friesen, W.; Hamza, H. A. Emulsification of Oil and Water in the Presence of Finely Divided Solids and Surface-Active Agents. Colloids Surf. 1984, 12 (3-4), 271-303.
27. Green, J. B.; Stierwalt, B. K.; Thomson, J. S.; Treese, C. A. Rapid isolation of carboxylic-acids from petroleum using high-performance liquid-chromatography. Anal. Chem. 1985, 57 (12), 2207-2211.
28. Koike, L.; Reboucas, L. M. C.; Reis, F. D. M.; Marsaioli, A. J.; Richnow, H. H.; Michaelis, W. Naphthenic acids from crude oils of Campos Basin. Org. Geochem. 1992, 18 (6), 851-860.