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15
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34047274896
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1a·3thf: 1H NMR (δ, C6D 6) 0.54 (s, 9H, 0.68 (s, 6H, 1.23 (m, 12H, 3.39 (m, 12H, 7LiNMR (δ, C6D6) 0.54. 1b-3thf: 1HNMR (δ, C6D6) 0.58 (s, 9H, 1.25 (m, 12H, 3.38 (m, 12H, 7.12-8.00 (m, 10H, 13CNMR (δ, C 6D6) 1.1, 25.4 (THF, 68.4 (THF, 124.4, 127.2, 137.0, 137.6; 7LiNMR (δ, C6D6) 0.36
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6) 0.36.
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-
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16
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34047253706
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2= 0.1576 (all data), GOF = 1.277.
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2= 0.1576 (all data), GOF = 1.277.
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17
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0001324136
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23
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34047257945
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Pt-P = 2788 Hz).
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Pt-P = 2788 Hz).
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-
-
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24
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34047248832
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2 = 0.2170 (all data), GOF = 1.345.
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2 = 0.2170 (all data), GOF = 1.345.
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25
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0035119573
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