Synthesis of TiO2 nanoparticles by hydrolysis and peptization of titanium isopropoxide solution

Journal of Materials Processing Technology

Volumn 189, Issue 1-3, 2007, Pages 296-300

  Mahshid, S ^a   Askari, M ^a   Ghamsari, M Sasani ^b  

^a University of Sharif   (Iran)

^b IRANIAN NATIONAL CENTER FOR LASER SCIENCE AND TECHNOLOGY   (Iran)

Author keywords

Crystallinity; Hydrolysis; Peptization; TiO2; Titanium isopropoxide

Indexed keywords

HYDROLYSIS; MORPHOLOGY; PARTICLE SIZE ANALYSIS; PH; SCANNING ELECTRON MICROSCOPY; SYNTHESIS (CHEMICAL); TITANIUM DIOXIDE; TRANSMISSION ELECTRON MICROSCOPY; X RAY DIFFRACTION;

CRYSTALLINITY; PEPTIZATION; RUTILE TRANSFORMATION; TITANIUM ISOPROPOXIDE;

NANOPARTICLES;

EID: 34047254664     PISSN: 09240136     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jmatprotec.2007.01.040     Document Type: Article

References (34)

1. Barbe C.J., Arendse F., Comte P., Jirousek M., and Grätzel M. Nanocrystalline titanium oxide electrodes for photovoltaic applications. J. Am. Ceram. Soc. 80 (1997) 3157
2. 2 nanoparticles: does it exist. Appl. Surf. Sci. 162-163 (2000) 565-570
3. 2 powders elaborated by sol-gel route and supercritical drying. Solar Energy Mater. Solar Cells 83 (2004) 421-433
4. Carp O., Huisman C.L., and Reller A. Photoinduced reactivity of titanium dioxide. Prog. Solid State Chem. 32 (2004) 133-177
5. 2 obtained by hydrothermal process for gas sensors. Sens. Actuators B: Chem. 103 (2004) 312-317
6. 2 nanoparticles in glycerol-containing solutions. Mater. Lett. 57 (2003) 2746-2750
7. (4-n)+ complexes. J. Colloid Interface Sci. 252 (2002) 339-346
8. 2 particles. J. Colloid Interface Sci. 252 (2002) 347-353
9. Arnal P., Corriu R.J.P., Leclercq D., Mutin P.H., and Vioux A. A solution chemistry study of nonhydrolytic sol-gel routes to titania. Chem. Mater. 9 (1997) 694-698
10. 2 in toluene by a solvothermal route. J. Cryst. Growth 254 (2003) 405-410
11. 2 in toluene with surfactant. J. Cryst. Growth 257 (2003) 309-315
12. 2 nanorods with nanotubes as the precursor. J. Phys. Chem. B 110 (2006) 4193-4198
13. Kolen'ko Y.V., Churagulov B.R., Kunst M., Mazerolles L., and Colbeau-Justin C. Photocatalytic properties of titania powders prepared by hydrothermal method. Appl. Catal. B: Environ. 54 (2004) 51-58
14. 2 synthesized by mechanical alloying. J. Alloys Compd. 375 (2004) 259-264
15. 2 powder with different grain sizes. Mater. Lett. 58 (2004) 513-515
16. 5 nanoparticles produced by ball-milling. J. Alloys Compd. 352 (2003) 16-20
17. Kamei M., and Mitsuhashi T. Hydrophobic drawings on hydrophilic surfaces of single crystalline titanium dioxide: surface wettability control by mechanochemical treatment. Surf. Sci. 463 (2000) L609-L612
18. 2 nanopowders using RF thermal plasma. Thin Solid Films 457 (2004) 186-191
19. 2 nanoparticles by pulsed laser ablation: ambient pressure dependence of crystallization. Jpn. J. Appl. Phys. 42 5A Pt 2 (2003) L479-L481
20. 2). Chem. Mater. 7 (1995) 1772-1778
21. Ding X.-Z., Qi Z.-Z., and He Y.-Z. Effect of hydrolysis water on the preparation of nano-crystalline titania powders via a sol-gel process. J. Mater. Sci. Lett. 14 (1995) 21-22
22. Vorkapic D., and Matsoukas T. Effect of temperature and alcohols in the preparation of titania nanoparticles from alkoxides. J. Am. Ceram. Soc. 81 (1998) 2815-2820
23. Look J.-L., and Zukoski C.F. Alkoxide-derived titania particles: use of electrolytes to control size and agglomeration levels. J. Am. Ceram. Soc. 75 (1992) 1587-1595
24. Look J.-L., Zukoski C.F., Look J.L., and Zukoski C.F. Colloidal stability of titania precipitate morphology: influence of short-range repulsions. J. Am. Ceram. Soc. 78 (1995) 21-32
25. 2 precursors prepared by peptization-hydrolysis method using polycarboxylic acid as peptizing agent. Mater. Chem. Phys. 56 (1998) 163-170
26. 2 nanaoparticles by the gel-sol method. 3: Formation process and size control. J. Colloidal Interface Sci. 259 (2003) 43-52
27. 2 nanaoparticles by the gel-sol method. 4: Shape control. J. Colloidal Interface Sci. 259 (2003) 53-61
28. Livage J., Henry M., and Sanchez C. Sol-gel chemistry of transition metal oxides. Prog. Solid State Chem. 18 (1988) 259-341
29. Sanchez C., Livage J., Henry M., and Babonneau F. Chemical modification of alkoxide precursors. J. Non-Cryst. Solids 100 (1988) 65-76
30. 2 nanoparticles in an acidic solution. Chem. Lett. 33 (2004) 1382-1383
31. 2 synthesized via sol-gel process. Microporous Mesoporous Mater. 166 (2003) 261-271
32. 2 nanoparticles from titanium (IV) alkoxide at high water/titanium ratio. J. Phys. Chem. B 107 (2003) 1734-1738
33. Ding X.Z., and Liu X.H. Grain growth enhanced by anatase to rutile transformation in gel-derived nanocrystalline titania powders. J. Alloys Compd. 248 (1997) 143-145
34. 2 powder. Mater. Chem. Phys. 78 (2002) 184-188