Synthesis, crystal structures, and photochromic properties of 6,6′ or 7,7′ or 6,7′-dimethyl-[2,2′-bi-1H-indene]-3,3′-diethyl-3,3′-dihydroxy-1,1′-diones

Tetrahedron

Volumn 63, Issue 20, 2007, Pages 4319-4327

  Chen, Yong ^a   Pang, Mei Li ^a   Cheng, Kai Ge ^a   Wang, Ying ^a   Han, Jie ^a   He, Zheng Jie ^a   Meng, Ji Ben ^a  

^a NANKAI UNIVERSITY   (China)

Author keywords

Crystal structure; Dimethyl 2,2 bi 1H indene diethyl 3,3 dihydroxy 1,1 diones; Organic solid material; Photochromism; Synthesis

Indexed keywords

4 METHYLPHTHALIC ANHYDRIDE; 6,6' DIMETHYL[2,2' BI 1H INDENE] 3,3' DIETHYL 3,3' DIHYDROXY 1,1' DIONE; 6,7' DIMETHYL[2,2' BI 1H INDENE] 3,3' DIETHYL 3,3' DIHYDROXY 1,1' DIONE; 7,7' DIMETHYL[2,2' BI 1H INDENE] 3,3' DIETHYL 3,3' DIHYDROXY 1,1' DIONE; ACID ANHYDRIDE; BIINDENYLIDENEDIONE DERIVATIVE; INDENE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; CRYSTAL STRUCTURE; CRYSTALLIZATION; ENANTIOMER; ISOMERISM; PRIORITY JOURNAL; RACEMIC MIXTURE; STRUCTURE ANALYSIS; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 34047247233     PISSN: 00404020     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tet.2007.03.030     Document Type: Article

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34. -3, reflection collected/unique 4679/1774 [R (int)=0.0720], final R indices [I>2σ(I)] R1=0.0897, wR2=0.2195, R indices (all data) R1=0.1247, wR=0.2496, GOF=1.019, CCDC 627736.